Study on dispersion behavior of submicron cerium oxide particles in concentrated suspensions by ultrasonic attenuation technique

Author(s):  
Zixin Luo ◽  
Qilong Wei ◽  
Qiang Yang ◽  
Wei Gao
2017 ◽  
Vol 24 (31) ◽  
pp. 24187-24200 ◽  
Author(s):  
Einstein Mariya David Sugantharaj David ◽  
Madhav Madurantakam Royam ◽  
Suresh Kumar Rajamani Sekar ◽  
Bhuvaneshwari Manivannan ◽  
Swathy Jalaja Soman ◽  
...  

2015 ◽  
Vol 645-646 ◽  
pp. 394-399
Author(s):  
Wei Gao ◽  
Qi Long Wei ◽  
Ling Ding ◽  
Xiao Yuan Li ◽  
Chao Wang ◽  
...  

A multi-scale method was developed, which utilized intrinsic relationships among zeta potential of particles, rheological properties of suspensions and particle size distribution (PSD), to analyze dispersion behavior of nanoparticles in concentrated suspensions. It was found that PSD of a kind of nanoceria particles by dynamic light scattering (DLS) method in solution A with concentration 5 wt% accorded well with that by direct TEM analysis, which meant the particles had been dispersed well. However, there had a significant difference when the concentration was increased to 20 wt%. When particles concentration increased from 5 wt% to 20 wt%, zeta potential in solution A changed from-150 mV to-100 mV, while zeta potential in solution B changed from-35mV to-45 mV. Variations of zeta potential of particles accorded well with rheological properties of suspensions too, from phenomenological models. When the suspensions composed by solution A and the nanoparticles with concentration about 20 wt% was diluted with its original solution to 5 wt%, the PSD of nanoceria could be measured indirectly, which accorded well with both that of a suspension prepared directly with near concentration and that from TEM images. Then a method to measure PSD of nanoparticles in concentrated suspension was brought forward.


RSC Advances ◽  
2014 ◽  
Vol 4 (2) ◽  
pp. 992-995 ◽  
Author(s):  
Mei Li ◽  
Yanhong Hu ◽  
Cuicui Liu ◽  
Jinguo Huang ◽  
Zhaogang Liu ◽  
...  

2013 ◽  
Vol 8 (6) ◽  
pp. 643-653 ◽  
Author(s):  
Ilse Gosens ◽  
Liesbeth E.A.M. Mathijssen ◽  
Bas G.H. Bokkers ◽  
Hans Muijser ◽  
Flemming R. Cassee

2010 ◽  
Vol 17 (02) ◽  
pp. 147-152 ◽  
Author(s):  
S. YIN ◽  
Y. MINAMIDATE ◽  
T. SATO

The morphological control of crystalline cerium oxide particles was realized by homogeneous precipitation process followed by calcination in air at 400°C. The effects of room temperature pre-aging time on the morphologies of final products were investigated. Monodispersed rod-like cerium carbonate precursor was produced at 70°C for 2 h using the solution without pre-aging treatment. In contrast, monodispersed spherical precursor and plate-like precursor were obtained under the same conditions after pre-aging the solution at 25°C for 72 and 144 h, respectively. Ceria particles with similar morphologies and particle size to those of carbonate precursor could be obtained after calcination in air at 400°C. The monodispersed spherical, rod-like, and plate-like cerium oxide particles were successfully synthesized.


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