scholarly journals Research on the method of quickly comparing the quality of Aluminium Powder for fireworks and firecrackers based on energy dispersive X-ray fluorescence spectrometer (EDXRF)

Author(s):  
Wu Jun-yi
2012 ◽  
Vol 67 (3) ◽  
pp. 235-242 ◽  
Author(s):  
A. Yu. Portnoi ◽  
G. V. Pavlinskii ◽  
M. S. Gorbunov ◽  
Yu. I. Sidorova

1977 ◽  
Vol 2 (4) ◽  
pp. 243-251 ◽  
Author(s):  
E. Laine ◽  
J. Kivilä ◽  
I. Lähteenmäki

The influence of preferred orientation on integrated x-ray intensities in powder specimen using energy-dispersive diffraction method is investigated. The theory used is based upon examination of the polar axis density distribution. The measurements were carried out using the Schulz technique added with defocusing correction. Experimental results are given for three aluminium powder specimens.


1975 ◽  
Vol 19 ◽  
pp. 253-265 ◽  
Author(s):  
J. M. Jaklevic ◽  
D. A. Landis ◽  
F. S. Goulding

An energy dispersive X-ray fluorescence spectrometer using pulsed X-ray excitation has been developed for use in large-scale environmental analysis programs. A grid controlled X-ray tube is coupled with variable secondary fluorescence targets to analyze for a wide variety of elements with almost optimum sensitivity. The operation of the pulsed tube in a feedback loop with the semiconductor detector spectrometer results in a substantial increase in output counting rates without pile-up. The loop functions by turning off the excitation immediately upon detection of an event by the spectrometer. Pileup events are virtually eliminated and the X-ray tube's available anode power is better utilized.The electronic control of this feedback mode results in some unique features in the response of the system to varying sample mass. These features are discussed in detail. Experimental results for sensitivity and accuracy over the range of elements measured are presented. Early operating experience with the unit indicates increases of counting rates of a factor of five compared with similar conventional systems.


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