Collaborative Study of Minerals in Feeds by Atomic Absorption Spectrophotometry

1968 ◽  
Vol 51 (4) ◽  
pp. 776-779 ◽  
Author(s):  
Mary Heckman
Keyword(s):  
Atomic Absorption ◽  
Collaborative Study ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Wet Digestion ◽  
Dry Ashing ◽  
Mineral Mixture ◽  
Determination Of Copper ◽  
Feed Samples

Abstract Eleven laboratories collaboratively studied the analysis of feeds for zinc, manganese, iron, and copper by atomic absorption spectrophotometry. Five feeds and one mineral mixture were analyzed. The feed samples were prepared by both dry ashing and wet digestion. Samples were analyzed chemically for manganese and iron. Results indicate the method is suitable for zinc, manganese, and iron. Further work is needed on the determination of copper. The method for atomic absorption analysis of feeds for calcium and magnesium (recommended too late for action in 1966) and the method for zinc, manganese, and iron are recommended for adoption as official, first action.

Minerals in Feeds by Atomic Absorption Spectrophotometry

1967 ◽  
Vol 50 (1) ◽  
pp. 45-50 ◽  
Author(s):  
Mary Heckman
Keyword(s):  
Sample Preparation ◽  
Atomic Absorption ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Wet Digestion ◽  
Dry Ashing ◽  
Mineral Mixture ◽  
Calcium Magnesium ◽  
Calcium And Magnesium

Abstract Seventeen laboratories collaborated in the study of analysis of feeds for calcium, magnesium, zinc, manganese, iron, and copper by atomic absorption spectrophotometry. Six feeds and one mineral mixture were analyzed; both dry ashing and wet digestion were used to prepare samples. Three feeds were in the form of solutions to eliminate sample preparation as a variable. Strontium and lanthanum were added to the feed to eliminate phosphorus interference and results were compared. Results indicate that the method is suitable for calcium and magnesium. Further work is needed on the determination of zinc, manganese, iron, and copper.

Collaborative Study Using Atomic Absorption Spectrophotometry for the Determination of Copper in Alcoholic Products

1967 ◽  
Vol 50 (2) ◽  
pp. 338-339
Author(s):  
Duane H Strunk ◽  
A A Andreasen
Keyword(s):  
Atomic Absorption ◽  
Spectrophotometric Method ◽  
Collaborative Study ◽  
Atomic Absorption Spectrophotometry ◽  
Good Precision ◽  
Absorption Method ◽  
Standard Curve ◽  
Absorption Spectrophotometry ◽  
Determination Of Copper

Abstract A collaborative study was conducted on the 'atomic absorption spectrophotometric method for measuring the concentration of copper in alcoholic products. In this method, the samples are aspirated directly into the burner of the instrument, and the absorhance values are converted to ppm copper by reference to a standard curve. Data show good precision and are comparable to those obtained by the ZDBT method. It is recommended that the atomic absorption method be adopted as official, first action.

Determination of Copper in Alfalfa

1971 ◽  
Vol 54 (4) ◽  
pp. 951-952
Author(s):  
A Donald Baker
Keyword(s):  
Sample Preparation ◽  
Atomic Absorption ◽  
Hydrofluoric Acid ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Dry Ashing ◽  
Wet Ashing ◽  
Aoac Method ◽  
Determination Of Copper

Abstract Copper in alfalfa is determined by atomic absorption spectrophotometry after dry-ashing or wet-ashing of the sample. The method is as precise as and considerably more rapid than the present AOAC method. The standard deviations of the method for wet- and dry-ashing sample preparation were 0.56 and 0.97%, respectively. Recovery of copper from spiked samples was 96—100%. Removal of silica by hydrofluoric acid fuming was not necessary.

Collaborative Study of Copper in Feeds by Atomic Absorption Spectrophotometry

1971 ◽  
Vol 54 (3) ◽  
pp. 666-668 ◽  
Author(s):  
Mary Heckman
Keyword(s):  
Atomic Absorption ◽  
Collaborative Study ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Wet Digestion ◽  
Dry Ashing

Abstract Eleven laboratories collaborated in a study of the analysis of copper in feeds by atomic absorption spectrophotometry. Four feeds containing varying levels of copper were prepared by several dry-ashing methods and by wet digestion. Results indicate that the method is satisfactory. The method has been adopted official first action.

Determination of Minor Nutrients in Fertilizers by Atomic Absorption Spectrophotometry: Second Collaborative Study

1965 ◽  
Vol 48 (6) ◽  
pp. 1100-1103
Author(s):  
C H Mcbride
Keyword(s):  
Atomic Absorption ◽  
Collaborative Study ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Method ◽  
Atomic Absorption Method ◽  
Absorption Spectrophotometry ◽  
Minor Nutrients

Abstract The atomic absorption method studied last year was re-examined and extended to include calcium and sodium. The procedures were submitted to 16 collaborators for determination of Ca, Cu, Fe, Mg, Mn, Na, and Zn. Results for Ca and Na were discouraging; further study is recommended.

Atomic Absorption Spectrophotometry: Determination of Chromium in Plants

1975 ◽  
Vol 58 (3) ◽  
pp. 433-435
Author(s):  
Earle E Cary ◽  
Oscar E Olson
Keyword(s):  
Atomic Absorption ◽  
Biological Materials ◽  
Atomic Absorption Spectrophotometry ◽  
Liquid Extraction ◽  
Absorption Spectrophotometry ◽  
Wet Digestion ◽  
Liquid Liquid Extraction ◽  
Chromium Recovery

Abstract A previously reported method for the determination of chromium in plants and biological materials has been simplified. The method, which involves wet digestion, isolation and concentration of chromium by liquid-liquid extraction, and final determination by atomic absorption spectrophotometry, is sensitive to about 20 ng chromium. Recovery studies and analysis of standard materials show that this method is reliable.

Atomic Absorption Spectrophotometric Method for Determination of Water-Soluble Copper in Water-Insoluble Copper Fungicides: CIPAC Collaborative Study. Comparison with Bathocuproine Method

1981 ◽  
Vol 64 (1) ◽  
pp. 75-78
Author(s):  
F Sánchez Rasero ◽  
◽  
P G Balayannis ◽  
H P Beyers ◽  
E Celma ◽  
...  
Keyword(s):  
Atomic Absorption ◽  
Collaborative Study ◽  
The United States ◽  
Atomic Absorption Spectrophotometry ◽  
Water Soluble ◽  
Absorption Spectrophotometry ◽  
Aas Method ◽  
Standard Deviations ◽  
The Difference

Abstract An atomic absorption spectrophotometric (AAS) method was collaboratively studied by 8 laboratories from Africa, the United States, Australia, and Europe. The samples were dispersed in deionized water. After centrifuging and filtering, the water-soluble copper in the filtrate was acidified and measured by atomic absorption spectrophotometry, in an airacetylene flame, at 324.7 nm. The results from 7 laboratories were satisfactory and no unfavorable comments were received. Repeatability standard deviations ranged from 0.005 to 0.023, and reproducibility standard deviations ranged from 0.012 to 0.062. When compared with the bathocuproine method, the difference in bias between both methods is not significant. They were both adopted as full CIPAC methods, with the bathocuproine method as the referee method. Both methods have been adopted official first action.

Determination of Mercury in Food Products and Biological Fluids by Aeration and Flameless Atomic Absorption Spectrophotometry

1971 ◽  
Vol 54 (1) ◽  
pp. 206-210 ◽  
Author(s):  
Virginia A Thorpe
Keyword(s):  
Atomic Absorption ◽  
Biological Fluids ◽  
Food Products ◽  
Atomic Absorption Spectrophotometry ◽  
Good Precision ◽  
Flameless Atomic Absorption ◽  
Absorption Spectrophotometry ◽  
Wet Digestion ◽  
Mercury In Fish

Abstract This paper describes a simple, rapid modification of a method developed at the Fisheries Research Board of Canada for determining mercury in fish and other food products. Wet digestion and flameless techniques of atomic absorption spectrophotometry are used. Replicate analyses on different days showed good precision and samples spiked with known amounts of mercury showed adequate recovery.

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