Determination of Cyclopiazonic Acid in Peanuts and Corn by Thin Layer Chromatography
1986 ◽
Vol 69
(6)
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pp. 964-966
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Keyword(s):
Abstract A thin layer chromatographic system including densitometry has been developed for determining cyclopiazonic acid in peanuts and corn. Samples are extracted with methanol-chloroform (20 + 80); the extract is stripped of most interferences by partitioning with aqueous sodium bicarbonate followed by acidification and repartitioning with chloroform. After thin layer chromatography and derivatization with dimethylaminobenzaldehyde- HCl spray, the toxin is quantitated by reflection densitometry at 540 nm. The recovery of cyclopiazonic acid averages 90% for peanuts and 85% for corn. The absolute detection limit is 25 ng per spot which translates to a detection limit of 125 μg/kg for a 50 g sample.
1990 ◽
Vol 73
(4)
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pp. 579-581
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1991 ◽
Vol 74
(4)
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pp. 655-660
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Keyword(s):
2016 ◽
Vol 29
(3)
◽
pp. 221-226
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2016 ◽
Vol 29
(3)
◽
pp. 190-194
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2017 ◽
Vol 30
(4)
◽
pp. 307-312