Room-temperature reactive bonding by using nano scale multilayer systems

Author(s):  
J. Braeuer ◽  
J. Besser ◽  
M. Wiemer ◽  
T. Gessner
2018 ◽  
Vol 2 (3) ◽  
pp. 31 ◽  
Author(s):  
Raquel Trujillano ◽  
Inés González-García ◽  
Alvaro Morato ◽  
Vicente Rives

Three series of layered double hydroxides (LDH) with a hydrotalcite-like structure and composition corresponding to [Mg4Al2(OH)12(CO3)]·3H2O have been prepared from a common batch by applying three different aging procedures, namely, stirring at room temperature, hydrothermal treatment, and microwave-hydrothermal treatment. It has been found that the tested properties of the samples (mainly related to their crystallinity) are considerably improved by using the microwave-hydrothermal treatment. Shorter times are also evinced than in the other two aging treatments; however, if the microwave-hydrothermal treatment is too far extended, incipient destruction of the particles is observed.


Author(s):  
I. Iniguez-de-la-Torre ◽  
V. Kaushal ◽  
M. Margala ◽  
T. Gonzalez ◽  
J. Mateos

MRS Advances ◽  
2018 ◽  
Vol 3 (44) ◽  
pp. 2713-2718 ◽  
Author(s):  
M M Saj Mohan ◽  
M V Sreenath ◽  
Ranjith Ramadurai

AbstractBiFeO3 (BFO) is the most studied room temperature multiferroic compound. In this work we demonstrate a template assisted growth process through which the growth strain is controlled to achieve required phase of BFO. Growth of (∼20nm) fully strained tetragonal (T), rhombohedral (R) and mixed phase of T and R of Bismuth ferrite (BiFeO3) was achieved by varying the thickness of the template layer. The different phases were confirmed by using high resolution x-ray diffractions studies. The conductivity map of all the three phases were carried out using an atomic force microscope operating in conductive mode. Tip induced surface defect migration within a given grain was observed in pure phases and the conductivity map confirmed the same. The room temperature resistivity is found to be decreasing systematically from 1.1×106 Ωm , 935×105 Ωm and 1.16×104 Ωm respectively for tetragonal, mixed phase and rhombohedral phase BFO. In the case of mixed phase both the nano- scale and macroscopic leakage current studies show low conductivity, which could be due to the increased pinning sites that increases the energy barrier for the defect migration. The local nano-scale measurements and conductivity mapping corroborates well with the macroscopic studies.


2017 ◽  
Vol 19 (20) ◽  
pp. 13101-13110 ◽  
Author(s):  
F. Lo Celso ◽  
Y. Yoshida ◽  
F. Castiglione ◽  
M. Ferro ◽  
A. Mele ◽  
...  

Neutron scattering patterns reveal fluorinated nano-scale domain segregation in fluorinated room temperature ionic liquids.


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