Creep Deformation Analysis of Grade 91 Steels and Prediction of Creep Strength Properties

Author(s):  
Kazuhiro Kimura ◽  
Kota Sawada ◽  
Hideaki Kushima

Creep deformation behavior was analyzed on Grade T91 steels and an empirical equation was derived to express creep strain as a function of time. Creep rupture life prediction was investigated by means of the derived empirical equation. Influence of creep rupture strain on creep rupture life predicted by the derived equation was small over a range of creep rupture strain from 0.05 to 0.30, especially creep rupture strain of 0.10 and above. Prediction accuracy of creep rupture life of the equation was better than that of creep rupture data analysis with a Larson-Miller parameter. Heat-to-heat variation of long-term creep rupture strength was appropriately observed. Minimum creep rate, onset of tertiary creep, and time to specific strain are easily predicted by the equation.

2017 ◽  
Vol 139 (5) ◽  
Author(s):  
K. Maruyama ◽  
N. Sekido ◽  
K. Yoshimi

Predictions as to 105 h creep rupture strength of grade 91 steel have been made recently. The predicted values are examined with long-term creep rupture data of the steel. Three creep rupture databases were used in the predictions: data of tube products of grade 91 steel reported in National Institute for Materials Science (NIMS) Creep Data Sheet (NIMS T91 database), data of T91 steel collected in Japan, and data of grade 91 steel collected by an American Society of Mechanical Engineers (ASME) code committee. Short-term creep rupture data points were discarded by the following criteria for minimizing overestimation of the strength: selecting long-term data points with low activation energy (multiregion analysis), selecting data points crept at stresses lower than a half of proof stress (σ0.2/2 criterion), and selecting data points longer than 1000 h (cutoff time of 1000 h). In the case of NIMS T91 database, a time–temperature parameter (TTP) analysis of a dataset selected by multiregion analysis can properly describe the long-term data points and gives the creep rupture strength of 68 MPa at 600 °C. However, TTP analyses of datasets selected by σ0.2/2 criterion and cutoff time of 1000 h from the same database overestimate the data points and predict the strength over 80 MPa. Datasets selected by the same criterion from the three databases provide similar values of the strength. The different criteria for data selection have more substantial effects on predicted values of the strength of the steel than difference of the databases.


Author(s):  
Kouichi Maruyama ◽  
Nobuaki Sekido ◽  
Kyosuke Yoshimi

Predictions as to 105 hrs creep rupture strength of grade 91 steel have been made recently. The predictions should be verified by some means, since they are based on certain assumptions. A formula for predicting long-term creep rupture lives should correctly describe long-term data points used in its formulation. Otherwise the formula cannot properly predict further longer-term creep rupture lives. On the basis of this consideration, the predictions are examined with long-term creep rupture data of the steel. In the predictions three creep rupture databases were used: data of tube products of grade 91 steel reported in NIMS Creep Data Sheet (NIMS T91 database), data of T91 steel collected in Japan, and data of grade 91 steel collected by an ASME code committee. Short-term creep rupture data points were discarded by the following criteria for minimizing overestimation of the strength: selecting long-term data points with low activation energy (multi-region analysis), selecting data points crept at stresses lower than a half of proof stress (σ0.2/2 criterion), and selecting data points longer than 1000 hrs (cut-off time of 1000 hrs). In the case of NIMS T91 database, a time-temperature parameter (TTP) analysis of a dataset selected by the multi-region analysis can properly describe the long-term data points. However, the TTP analyses of datasets selected by the σ0.2/2 criterion and by the cut-off time of 1000 hrs from the same database overestimate the long-term data points. The different criteria for data selection have more substantial effects on predicted values of the strength of the steel than difference of the databases.


Author(s):  
Walter Bendick ◽  
Jean Gabrel ◽  
Bruno Vandenberghe

The application of new heat resistant steels in power plants requires reliable long term creep rupture strength values as basis for design. Modern martensitic 9% Cr-steels have complex microstructures that change with service exposure. That is why extrapolations of long term strength properties will be most difficult. Due to new long term test results, re-assessments became necessary for grades 911 and 92. Different methods have been used. Good agreement was obtained between a graphical and the numerical ISO 6303 method. In both cases a two-step assessment procedure was used. First the raw data was prepared in a suitable way, which was followed by mathematical averaging procedures. For comparison a Larson-Miller analysis on the raw data was performed, too. The results turned out to be too optimistic at temperatures higher than 575°C (1050°F). It is shown that a suitable preparation of data can improve the Larson-Miller assessment. As a result of the new assessments the design values had to be reduced for both grades. With respect to previous assessments the new values are up to almost 10% lower. In the case of grade 92 the difference from the former ASME values are even higher. Consequences concerning design and service operation are discussed.


Author(s):  
Masatsugu Yaguchi ◽  
Kaoru Nakamura ◽  
Sosuke Nakahashi

Creep rupture data of welded joints of ASME Grade 91 type steel have been collected from Japanese plants, milling companies and institutes, and the long-term creep rupture strength of the material has been evaluated. This evaluation of welded joints of Grade 91 steel is the third one in Japan as similar studies were conducted in 2004 and 2010. The re-evaluation of the creep rupture strength was conducted with emphasis on the long-term creep rupture data obtained since the previous study, with durations of the new data of up to about 60000h. The new long-term data exhibited lower creep strength than that obtained from the master creep life equation for welded joints of Grade 91 steel determined in 2010, then the master creep life equation was again reviewed on the basis of the new data using the same regression method as that used in 2010. Furthermore, the weld strength reduction factors obtained from 100000h creep strength of welded joints and the base metals are given as a function of temperature, where the master creep equations of the base metals are also redetermined in this study.


Author(s):  
Kazuhiro Kimura ◽  
Kota Sawada ◽  
Masakazu Fujitsuka ◽  
Hideaki Kushima

Creep test of ASME Grade 23 steel has been conducted at 625 and 650°C in helium gas atmosphere. Long-term creep strength of the steel in helium gas was compared with that in air and the influence of oxidation on long-term creep strength was investigated. Creep rupture strength drop was observed in the long-term at 625 and 650°C in air, and the same creep rupture strength drop was observed also in helium gas at 625°C. On the other hand, although creep rupture strength drop was observed in the long-term at 650°C in helium gas, creep rupture life in the long-term in helium gas was slightly longer than that in air at 650°C. Creep rupture life in the long-term at 650°C in air is reduced by not only degradation due to microstructural change, but also marked oxidation, however, that at 625°C is considered to be shortened mainly by a degradation caused by microstructural change. Long-term creep strength of ASME Grade 23 steel at 600°C and above should be reevaluated in consideration of strength drop due to microstructural change.


Author(s):  
Kazuhiro Kimura ◽  
Masatsugu Yaguchi

Creep rupture strength of ASME Grades 91, 92, 122 and 23 type steels were evaluated by the SHC committee in 2004 and 2005, and the Assessment Committee on Creep Data of High Chromium Steels in 2010. According to the evaluation of creep rupture strength, allowable stress of the steels was revised and weld strength reduction factor (WSRF) was established. In 2015, the creep rupture data of those steels was collected from materials producers, power plant manufacturers and institutes in Japan and a review of long-term creep rupture strength of the steels was conducted by the Assessment Committee on Creep Data of High Chromium Steels in reference to the previous evaluation. It has been confirmed with the latest dataset that re-evaluation of long-term creep rupture strength is not required for Grades 92, 122 and 23 type steels. On the other hand, lower creep rupture strength compared with the previous evaluation was recognized on the new creep rupture data of Grade 91 steels, therefore, re-evaluation of creep rupture strength was conducted on Grade 91 steels. Creep rupture strength was assessed by means of region splitting analysis method in consideration of 50% of 0.2% offset yield strength, in the same way as the previous study. According to the evaluation of long-term creep strength of the steels, allowable tensile stress was reviewed and proposed revision was concluded.


Author(s):  
Kazuhiro Kimura ◽  
Kota Sawada

Abstract Creep deformation behavior, creep strength property and microstructural evolution during creep exposure were investigated on Super 304H steel for boiler tube. In the high stress and lower temperature regime, creep rupture strength of Super 304H steel is higher than that of SUS304H steel. The slope of stress vs. time to rupture curve of Super 304H steel, however, becomes steeper with increases in creep exposure time and temperature, and the creep rupture strength of Super 304H steel becomes closer to that of SUS304H steel after the tens of thousands of hours at 700°C (1292°F) and above. In the short-term, at 600°C (1112°F), creep rupture ductility increases with increase in creep rupture life. However, it tends to decrease after showing this maximum value and the creep rupture ductility decreases with increase in temperature. The complex shape of creep rate vs. time curves, with two minima in creep rate, was observed at 600°C (1112°F). Several type precipitates of niobium carbonitride (Nb(C,N)), Z phase (NbCrN), and copper were observed in Super 304H steel, as well as M23C6 carbide and sigma phase observed in SUS304H steel. The change in slope of stress vs. time to rupture curve is caused by disappearance of precipitation strengthening effect during creep exposure. Accuracy of creep rupture life evaluation was improved by stress range splitting method which takes into account the change in slope of stress vs. time to rupture curves was demonstrated.


Author(s):  
Kazuhiro Kimura ◽  
Kota Sawada

Abstract Creep deformation behavior, creep strength property and microstructural evolution during creep exposure were investigated on Super 304H steel for boiler tube. In the high stress and lower temperature regime, creep rupture strength of Super 304H steel is higher than that of SUS304H steel. The slope of stress vs. time to rupture curve of Super 304H steel, however, becomes steeper with increase in creep exposure time and temperature, and the creep rupture strength of Super 304H steel becomes closer to that of SUS304H steel after the tens of thousands of hours at 700°C and above. In the short-term, at 600°C, creep rupture ductility increases with increase in creep rupture life. However, it tends to decrease after showing the maximum value and the creep rupture ductility decreases with increase in temperature. The complex shape of creep rate vs. time curves, with two minima in creep rate, was observed at 600°C. Several type precipitates of niobium carbonitride (Nb(C,N)), Z phase (NbCrN), and copper were observed in Super 304H steel, as well as M23C6 carbide and sigma phase observed in SUS304H steel. The change in slope of stress vs. time to rupture curve is caused by disappearance of precipitation strengthening effect during creep exposure. Accuracy of creep rupture life evaluation was improved by stress range splitting method which takes into accounts of the change in slope of stress vs. time to rupture curves was demonstrated.


2006 ◽  
Vol 129 (3) ◽  
pp. 449-453 ◽  
Author(s):  
Kouichi Maruyama ◽  
Kyosuke Yoshimi

Long-term creep rupture life is usually evaluated from short-term data by a time-temperature parameter (TTP) method. The allowable stress of Gr.122 steel listed in the ASME code has been evaluated by this method and is recognized to be overestimated. The objective of the present study is to understand the causes of the overestimation and propose appropriate methodology for avoiding the overestimation. The apparent activation energy Q for rupture life of the steel changes from a high value of short-term creep to a low value of long-term creep. However, the decrease in Q is ignored in the conventional TTP analyses, resulting in the overestimation of rupture life. A multiregion analysis of creep rupture data is employed to avoid the overestimation; in the analysis creep rupture data are divided into a couple of regions so that the Q value is unique in each divided region. The multiregion analysis provides a good fit to the data and the lowest value of 105h creep rupture strength among the three ways of data analysis examined. A half of 0.2% proof stress cannot provide an appropriate boundary for dividing data to be used in the multiregion analysis. In the 2001 edition of the ASME code an F average concept has been proposed as a substitution for the safety factor of 2∕3 for average rupture stress. The allowable stress of Gr.122 steel changes significantly depending on the allowable stress criteria as well as the methods of rupture data analysis: i.e., from 74MPato48MPa.


2007 ◽  
Vol 561-565 ◽  
pp. 163-166
Author(s):  
Yoshihiro Terada ◽  
Tatsuo Sato

Creep rupture tests were performed for a die-cast Mg-Al-Ca alloy AX52 (X representing calcium) at 29 kinds of creep conditions in the temperature range between 423 and 498 K. The creep curve for the alloy is characterized by a minimum in the creep rate followed by an accelerating stage. The minimum creep rate (ε& m) and the creep rupture life (trup) follow the phenomenological Monkman-Grant relationship; trup = C0 /ε& m m. It is found for the AX52 die-cast alloy that the exponent m is unity and the constant C0 is 2.0 x 10-2, independent of creep testing temperature. The values of m and C0 are compared with those for another die-cast magnesium alloys. The value m=1 is generally detected for die-cast magnesium alloys. On the contrary, the value of C0 sensitively depends on alloy composition, which is reduced with increasing the concentration of alloying elements such as Al, Zn and Ca.


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