The nuclear Overhauser effect between phosphorus and hydrogen in selected organo phosphorus compounds

H. Beierbeck; R. Martino; John K. Saunders; Claude Benezra

doi:10.1139/v76-275

The nuclear Overhauser effect between phosphorus and hydrogen in selected organo phosphorus compounds

Canadian Journal of Chemistry ◽

10.1139/v76-275 ◽

1976 ◽

Vol 54 (12) ◽

pp. 1918-1922 ◽

Cited By ~ 6

Author(s):

H. Beierbeck ◽

R. Martino ◽

John K. Saunders ◽

Claude Benezra

Keyword(s):

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Dipole Interaction ◽

Lattice Relaxation Time ◽

Spin Lattice Relaxation ◽

Phosphorus Compounds ◽

Spin Lattice ◽

Overhauser Effect ◽

Internuclear Distances ◽

Nuclear Overhauser

The nuclear Overhauser effect (nOe) observed between phosphorus and hydrogen together with carbon and phosphorus spin lattice relaxation time (T1) data are presented for a number of phosphorus containing compounds. The dominant mechanism for phosphorus relaxation is shown to be the dipole-dipole interaction between phosphorus and hydrogen. From the nOe and T1 data the determination of phosphorus–hydrogen internuclear distances is demonstrated.

Reliability of 1H and 13C NMR measurement. Spin-lattice relaxation time and nuclear Overhauser effect.

Kobunshi ◽

10.1295/kobunshi.38.292 ◽

1989 ◽

Vol 38 (4) ◽

pp. 292-293

Author(s):

FUMITAKA HORII

Keyword(s):

Relaxation Time ◽

13C Nmr ◽

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Lattice Relaxation Time ◽

Spin Lattice Relaxation ◽

1H And 13C Nmr ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

ChemInform Abstract: Use of Proton Spin-Lattice Relaxation and Nuclear Overhauser Effect Data in Structure Analysis of Alkaloids.

Chemischer Informationsdienst ◽

10.1002/chin.198642047 ◽

1986 ◽

Vol 17 (42) ◽

Author(s):

W. J. CHAZIN ◽

L. D. COLEBROOK

Keyword(s):

Structure Analysis ◽

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Proton Spin ◽

Spin Lattice Relaxation ◽

Effect Data ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

Use of proton spin-lattice relaxation and nuclear Overhauser effect data in structure analysis of alkaloids

The Journal of Organic Chemistry ◽

10.1021/jo00358a015 ◽

1986 ◽

Vol 51 (8) ◽

pp. 1243-1253 ◽

Cited By ~ 19

Author(s):

Walter J. Chazin ◽

Lawrence D. Colebrook

Keyword(s):

Structure Analysis ◽

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Proton Spin ◽

Spin Lattice Relaxation ◽

Effect Data ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

A 31P-NMR spin-lattice relaxation and 31P{1H} nuclear Overhauser effect study of sonicated small unilamellar phosphatidylcholine vesicles

Biochimica et Biophysica Acta (BBA) - Biomembranes ◽

10.1016/0005-2736(92)90142-9 ◽

1992 ◽

Vol 1104 (1) ◽

pp. 137-146 ◽

Cited By ~ 8

Author(s):

Joseph S. Tauskela ◽

Michael Thompson

Keyword(s):

31P Nmr ◽

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Effect Study ◽

Spin Lattice Relaxation ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

Hydrocarbon chain conformation of bipolar surfactants in micelles. A magnetic field-dependent carbon-13 and nitrogen-14 NMR spin-lattice relaxation and nuclear Overhauser effect study of N,N'-1,20-eicosanediylbis(triethylammonium bromide)

The Journal of Physical Chemistry ◽

10.1021/j100349a036 ◽

1989 ◽

Vol 93 (12) ◽

pp. 4861-4867 ◽

Cited By ~ 22

Author(s):

Tuck. C. Wong ◽

K. Ikeda ◽

K. Meguro ◽

O. Soederman ◽

U. Olsson ◽

...

Keyword(s):

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Hydrocarbon Chain ◽

Effect Study ◽

Spin Lattice Relaxation ◽

Spin Lattice ◽

Overhauser Effect ◽

Field Dependent ◽

Nuclear Overhauser ◽

Triethylammonium Bromide

Molecular dynamics in sodium dodecyl sulfate micelles elucidated using carbon-13 and proton spin-lattice relaxation, carbon-13 spin-spin relaxation, and proton nuclear Overhauser effect spectroscopy

The Journal of Physical Chemistry ◽

10.1021/j100285a030 ◽

1987 ◽

Vol 91 (1) ◽

pp. 131-137 ◽

Cited By ~ 14

Author(s):

Jeffrey F. Ellena ◽

Raymond N. Dominey ◽

David S. Cafiso

Keyword(s):

Molecular Dynamics ◽

Sodium Dodecyl Sulfate ◽

Nuclear Overhauser Effect ◽

Sodium Dodecyl ◽

Lattice Relaxation ◽

Proton Spin ◽

Spin Lattice Relaxation ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

ChemInform Abstract: MICELLAR DYNAMICS AND ORGANIZATION. A MULTIFIELD CARBON-13 NMR SPIN-LATTICE RELAXATION AND (PROTON) CARBON-13 NUCLEAR OVERHAUSER EFFECT STUDY

Chemischer Informationsdienst ◽

10.1002/chin.198431057 ◽

1984 ◽

Vol 15 (31) ◽

Author(s):

H. WALDERHAUG ◽

O. SOEDERMAN ◽

P. STILBS

Keyword(s):

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Effect Study ◽

Spin Lattice Relaxation ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

Anisotropy of local relaxation properties of macromolecules. Spin-lattice relaxation of 13C nuclei, the nuclear overhauser effect and the estimation of parameters of an equivalent ellipsoid for kinetic segments of polymer chains

Die Makromolekulare Chemie Theory and Simulations ◽

10.1002/mats.1993.040020102 ◽

1993 ◽

Vol 2 (1) ◽

pp. 13-20 ◽

Cited By ~ 3

Author(s):

Yuli Ya. Gotlib ◽

Isaak A. Torchinski ◽

Vladimir A. Shevelev

Keyword(s):

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Polymer Chains ◽

Spin Lattice Relaxation ◽

Estimation Of Parameters ◽

Relaxation Properties ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser ◽

Local Relaxation

Micellar dynamics and organization. A multifield carbon-13 NMR spin-lattice relaxation and {proton} carbon-13 nuclear Overhauser effect study

The Journal of Physical Chemistry ◽

10.1021/j150652a043 ◽

1984 ◽

Vol 88 (8) ◽

pp. 1655-1662 ◽

Cited By ~ 65

Author(s):

Harald Walderhaug ◽

Olle Soederman ◽

Peter Stilbs

Keyword(s):

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Effect Study ◽

Spin Lattice Relaxation ◽

Spin Lattice ◽

Overhauser Effect ◽

Nuclear Overhauser

Relaxation pathway analysis by 1H spin-lattice relaxation and nuclear Overhauser effect difference measurements. Application to a reassignment of the 1H nmr spectrum of strychnine and to the determination of the structure and stereochemistry of some strychnine sulfonic acids

Canadian Journal of Chemistry ◽

10.1139/v83-299 ◽

1983 ◽

Vol 61 (8) ◽

pp. 1749-1755 ◽

Cited By ~ 15

Author(s):

Walter J. Chazin ◽

Lawrence D. Colebrok ◽

John T. Edward

Keyword(s):

Pathway Analysis ◽

Nuclear Overhauser Effect ◽

Lattice Relaxation ◽

Coupling Constants ◽

Spin Lattice Relaxation ◽

Sulfonic Acids ◽

Spin Lattice ◽

Overhauser Effect ◽

Effect Difference ◽

Nuclear Overhauser

The 1H relaxation pathway analysis of strychnine and some strychnine sulfonic acids has been carried out by spin-lattice relaxation and nuclear Overhauser effect difference measurements. Some previously reported 1H chemical shifts and coupling constants for strychnine are shown to be in error. New assignments for positions 15, 17, 18, and 20 have been made. Proposed sites of substitution of the sulfonic acids have been verified, and the previously undetermined stereochemistry of one of the acids has been established.