FORMATION OF COLLOIDAL GOLD NANOPARTICLES BY USING FEMTOSECOND LASER ABLATION

2009 ◽  
Vol 08 (01n02) ◽  
pp. 209-212 ◽  
Author(s):  
M. A. SOBHAN ◽  
M. AMS ◽  
M. J. WITHFORD ◽  
E. M. GOLDYS

Colloidal gold nanoparticles were produced by irradiating a gold disc with a femtosecond laser beam in pure deionized water. Variation of laser fluence between 38 and 330 J/cm2 was used to control the nanoparticle size distribution. The nanoparticles produced were spherically shaped with average diameter between 9 and 10 nm. The effect of ablation time on the nanoparticle production efficiency and size distribution was also studied.

2011 ◽  
Vol 362 (2) ◽  
pp. 325-329 ◽  
Author(s):  
Tetsuro Soejima ◽  
Seisaku Oshiro ◽  
Yasuji Nakatsuji ◽  
Seishiro Ito

2011 ◽  
Vol 26 (8) ◽  
pp. 3700-3704 ◽  
Author(s):  
Yu Zhou ◽  
Xiang-Li Tian ◽  
Yan-Song Li ◽  
Feng-Guang Pan ◽  
Yuan-Yuan Zhang ◽  
...  

2015 ◽  
Vol 1115 ◽  
pp. 386-389
Author(s):  
Haroon Haiza ◽  
I.I. Yaacob ◽  
Ahmad Zahirani Ahmad Azhar

Colloidal gold nanoparticles have been successfully prepared using a simple two-electrode cells connected to a DC power supply. During the electro-dissolution-reduction process, the bulk gold at the anode oxidized into gold cations which then reacted with the chloride ions to form aurochloride complex. The complex ions were then reduced by the citrate ion to form colloidal gold nanoparticles. The size and shape of the nanoparticles were modulated by varying the terminal voltages. The colloidal gold nanoparticles obtained were characterized by field-emission scanning electron microscope (FESEM), transmission electron microscope (TEM) and ultraviolet-visible spectrophotometer (UV-Vis). From FESEM analysis, it was found that by increasing the voltage, the size of colloidal gold nanoparticles produced marginally decreased. The mean sizes of gold nanoparticles were roughly about 23.5 nm, 23.2 nm and 19.3 nm for 32 V, 36 V and 40 V, respectively. TEM micrograph showed that the shape of gold nanoparticles obtained is almost spherical. The characteristic peaks of UV-Vis spectra revealed that the suspension was indeed colloidal gold nanoparticles. Keywords: Gold, Nanoparticles, Electro-dissolution-reduction


2012 ◽  
Vol 51 (32) ◽  
pp. 8122-8122 ◽  
Author(s):  
Hong Wang ◽  
Liyong Chen ◽  
Xiaoshuang Shen ◽  
Liangfang Zhu ◽  
Jiating He ◽  
...  

2021 ◽  
Author(s):  
Junjun Cao ◽  
Jie Zhang ◽  
Ning Yuan ◽  
Yixiao Sun ◽  
Zhihua Xu ◽  
...  

Abstract Research on the activity of nanoenzymes has always been a focus of nanomaterials. In this study, several reducing agents with different structures were used to prepare colloidal gold with a negative charge and similar size by controlling the temperature and pH. The affinity analysis of the substrate H 2 O 2 and TMB showed that the activity of colloidal gold nanoenzymes prepared by different reducing agents was in the order of Cc, Hq, Rs, Vc, Ga, Sc, Sm, St. The rule is that the enzyme activity of colloidal gold reduced by benzene ring is higher than that of colloidal gold enzyme reduced by linear chain. Finally, we discussed the activity of colloidal gold peroxidase from the number and position of isomers and functional groups, and demonstrated that the nanoenzyme activity affected the surface activity of colloidal gold, the elimination of hydroxyl radical and TMB binding efficiency.


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