scholarly journals X-ray powder diffraction analysis of a new palladium(II) amino acid complex

2004 ◽  
Vol 19 (3) ◽  
pp. 270-271 ◽  
Author(s):  
Pedro P. Corbi ◽  
Antonio C. Massabni ◽  
Claudio M. Costa-Neto
Keyword(s):  
Amino Acid ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Acid Complex ◽  
X Ray ◽  
Cell Parameters ◽  
Amino Acid Complex ◽  
Orthorhombic Cell

Powder X-ray diffraction data for a new palladium(II) amino acid complex, of composition PdC12H20N2O4S2, are presented in this paper. Orthorhombic cell parameters are: a=10.740 Å, b=19.999 Å, and c=5.2470 Å. © 2004 International Centre for Diffraction Data.

scholarly journals X-ray powder diffraction analysis of methionine sulfoxide

2001 ◽  
Vol 16 (3) ◽  
pp. 163-164
Author(s):  
Pedro P. Corbi ◽  
Petr Melnikov ◽  
Antonio C. Massabni
Keyword(s):  
Amino Acid ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Methionine Sulfoxide ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cell Parameters ◽  
Monoclinic Cell

Powder X-ray diffraction data for methionine sulfoxide, C5H11NO3S, obtained from the commercial amino acid, are presented in this work. Monoclinic cell parameters are: a=15.500 Å; b=3.820 Å; c=13.490 Å; β=97.300 °.

scholarly journals Powder X-ray characterization of djenkolic acid

2001 ◽  
Vol 16 (1) ◽  
pp. 46-47
Author(s):  
Petr Melnikov ◽  
Alexandre Cuin ◽  
Pedro P. Corbi ◽  
Maurício Cavicchioli ◽  
Antonio C. Massabni
Keyword(s):  
Amino Acid ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Natural Amino Acid ◽  
Powder Diffraction Data ◽  
X Ray ◽  
Cell Parameters ◽  
Orthorhombic Cell ◽  
Djenkolic Acid

X-ray powder diffraction data for the orthorhombic natural amino acid djenkolic acid, C7H14N2O4S2, is described in this paper. The orthorhombic cell parameters are: a=8.12 Å, b=12.16 Å, and c=5.38 Å

X-ray powder diffraction analysis of tegafur

2006 ◽  
Vol 21 (3) ◽  
pp. 245-247 ◽  
Author(s):  
F. Needham ◽  
J. Faber ◽  
T. G. Fawcett ◽  
D. H. Olson
Keyword(s):  
Single Crystal ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Antineoplastic Agent ◽  
X Ray Diffraction ◽  
Triclinic Crystal System ◽  
X Ray ◽  
Cell Parameters ◽  
Structural Database

An experimental X-ray powder diffraction pattern was produced and analyzed for alpha-polymorphic tegafur, also called Ftorafur (an antineoplastic agent). The indexed data matched the powder patterns in the ICDD PDF-4/Organics database calculated from the reported single-crystal X-ray diffraction data in the Cambridge Structural Database. Alpha tegafur has a triclinic crystal system, with reduced cell parameters of a=16.720(6) Å, b=9.021(5) Å, c=5.995(3) Å, α=93.66(4)°, β=93.15(8)°, γ=100.14(4)°. There are four formula units contained in one unit cell. The cell volume and space group were determined to be 886.27 Å3 and P-1, respectively.

Powder X-Ray Diffraction Data for Ca2Bi2O5and C4Bi6O13

1992 ◽  
Vol 7 (2) ◽  
pp. 109-111 ◽  
Author(s):  
C.J. Rawn ◽  
R.S. Roth ◽  
H.F. McMurdie
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Neutron Powder Diffraction ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray ◽  
Cell Dimensions ◽  
Powder Samples ◽  
Orthorhombic Cell ◽  
Unit Cell Dimensions

AbstractSingle crystals and powder samples of Ca2Bi5O5and Ca4Bi6O13have been synthesized and studied using single crystal X-ray diffraction as well as X-ray and neutron powder diffraction. Unit cell dimensions were calculated using a least squares analysis that refined to a δ2θof no more than 0.03°. A triclinic cell was found with space group , a = 10.1222(7), b = 10.1466(6), c = 10.4833(7) Å. α= 116.912(5), β= 107.135(6) and γ= 92.939(6)°, Z = 6 for the Ca2Bi2O5compound. An orthorhombic cell was found with space group C2mm, a = 17.3795(5), b = 5.9419(2) and c = 7.2306(2) Å, Z = 2 for the Ca4Bi6O13compound.

X-ray-diffraction data of Pb2(C2O4)(NO3)2·2H2O

1996 ◽  
Vol 11 (1) ◽  
pp. 7-8 ◽  
Author(s):  
Hee-Lack Choi ◽  
Nobuo Ishizawa ◽  
Naoya Enomoto ◽  
Zenbe-e Nakagawa
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters ◽  
Crystal System

X-ray powder-diffraction data for Pb2(C2O4)(NO3)2·2H2O were obtained. The crystal system was determined to be monoclinic. The unit-cell parameters were refined to a=10.613(2) Å, b=7.947(2) Å, c=6.189(1) Å, and β=104.48(2)°.

Synthesis and powder X-ray diffraction data of a new iron phosphate Fe(PO4)·0.5H2O

1998 ◽  
Vol 13 (4) ◽  
pp. 246-248 ◽  
Author(s):  
Nubuo Ishizawa ◽  
Atsushi Saiki ◽  
Kyoji Ohdan ◽  
Mamoru Ai
Keyword(s):  
Water Vapor ◽  
Oxalic Acid ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Iron Phosphate ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters

X-ray powder-diffraction data were collected for a new iron phosphate, Fe(PO4)·0.5H2O, obtained by reducing FePO4 with oxalic acid at 220 °C in the presence of water vapor and oxygen. The crystal system was determined to be orthorhombic with unit-cell parameters a=15.991(6) Å, b=20.156(7) Å, and c=7.223(2) Å.

X-ray diffraction analysis of (Na0.6H0.4)(Ta0.7Nb0.3)O3

1999 ◽  
Vol 14 (3) ◽  
pp. 231-233 ◽  
Author(s):  
Raj P. Singh ◽  
Michael J. Miller ◽  
Jeffrey N. Dann
Keyword(s):  
High Temperature ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
Type Structure ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
X Ray

(Na0.6H0.4)(Ta0.7Nb0.3)O3 was synthesized by heating a tantalum/niobium scale containing two sodium tantalate/niobate phases :Na14(Ta0.7Nb0.3)12O37·31H2O and NaH2Ta0.7Nb0.3O4. Powder X-ray diffraction data for (Na0.6H0.4)(Ta0.7Nb0.3)O3 indicated it to be a cubic perovskite (ABO3/ReO3 type structure) with unit cell a0=3.894 Å. The compound is analogous to the mineral lueshite (NaNbO3), and to the high temperature forms of NaTaO3 and NaNbO3. Powder diffraction data for (Na0.6H0.4)(Ta0.7Nb0.3)O3 will be useful in the analysis of synthetic tantalum/niobium concentrates.

X-ray diffraction data of Ti2O2(C2O4)(OH)2·H2O

1994 ◽  
Vol 9 (3) ◽  
pp. 187-188 ◽  
Author(s):  
Hee-Lack Choi ◽  
Naoya Enomoto ◽  
Nobuo Ishizawa ◽  
Zenbe-e Nakagawa
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Space Group ◽  
X Ray ◽  
Cell Parameters ◽  
Crystal System

X-ray powder diffraction data for Ti2O2(C2O4)(OH)2·H2O were obtained. The crystal system was determined to be orthorhombic with space group C2221. The unit cell parameters were refined to a = 1.0503(2) nm, b = 1.5509(3) nm, and c = 0.9700(1) nm.

X-ray powder diffraction analysis of imipenem monohydrate

2012 ◽  
Vol 27 (1) ◽  
pp. 20-24
Author(s):  
F. Needham ◽  
C. E. Crowder ◽  
J. W. Reid ◽  
T. G. Fawcett ◽  
J. Faber
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Orthorhombic Crystal ◽  
X Ray ◽  
Cell Parameters ◽  
Pharmaceutical Agent ◽  
Structural Database

An experimental X-ray powder diffraction pattern was produced and analyzed for imipenem monohydrate, an antimicrobial pharmaceutical agent. Although there are no experimental powder patterns in the ICDD PDF-4/Organics Database, there is one powder pattern calculated with single-crystal X-ray diffraction data from the Cambridge Structural Database. Here, we report the refined experimental powder diffraction data for imipenem monohydrate. These data for imipenem monohydrate are consistent with an orthorhombic crystal system having reduced unit-cell parameters of a = 8.2534(3) Å, b = 11.1293(4) Å, and c = 15.4609(6) Å. The resulting unit-cell volume, 1420.15(15) Å3, indicates four formula units per unit cell. Observed peaks are consistent with the P212121 space group.

X-ray powder diffraction data of lapatinib ditosylate monohydrate

2009 ◽  
Vol 24 (3) ◽  
pp. 250-253 ◽  
Author(s):  
Peter Varlashkin
Keyword(s):  
Breast Cancer ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Room Temperature ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters ◽  
Diffraction Structure

The room temperature powder pattern of lapatinib ditosylate monohydrate (active ingredient in Tykerb used to treat refractory breast cancer) was indexed and the cell from the single crystal X-ray diffraction structure was refined using the experimental capillary data. Unit-cell parameters for the orthorhombic compound with space group Pbca refined from powder diffraction data are a=9.6850±0.0009 Å, b=29.364±0.003 Å, and c=30.733±0.003 Å, α=β=γ=90°, z=8, V=8740.1 Å3. Values of 2θ, d, I, and Miller indices are reported.

Sign in / Sign up

Export Citation Format

Share Document