Microwave Assisted Hydrothermal Method for Porous Zinc Oxide Nanostructured-Films

2013 ◽  
Vol 13 (4) ◽  
pp. 2667-2674 ◽  
Author(s):  
Noor J. Ridha ◽  
Akrajas Ali Umar ◽  
F. Alosfur ◽  
Mohammad Hafizuddin Haji Jumali ◽  
Muhamad Mat Salleh
2019 ◽  
Vol 18 (03n04) ◽  
pp. 1940045 ◽  
Author(s):  
E. Chubenko ◽  
I. Gerasimenko ◽  
V. Bondarenko ◽  
D. Zhigulin

ZnO nanostructured films doped with Co and Ni deposited by hydrothermal method on silicon substrates covered with undoped ZnO sublayer were studied. SEM images of the films demonstrated them to consist of densely packed vertical nanopillars. Doping ZnO films with Ni or Co at concentrations up to [Formula: see text][Formula: see text]cm[Formula: see text] quenches their UV-excited photoluminescence. The doping also leads to the slight ferromagnetic behavior of ZnO.


2013 ◽  
Vol 3 (4) ◽  
pp. 477-484
Author(s):  
Arnayra Silva ◽  
Jefferson Andrade ◽  
Graziela Casali ◽  
Severino Lima ◽  
Elson Longo ◽  
...  

2019 ◽  
Vol 21 (5) ◽  
Author(s):  
I. A. Garduño-Wilches ◽  
G. Alarcón-Flores ◽  
S. Carmona-Téllez ◽  
J. Guzmán ◽  
M. Aguilar-Frutis

Crystals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1040 ◽  
Author(s):  
Getachew Solomon ◽  
Raffaello Mazzaro ◽  
Vittorio Morandi ◽  
Isabella Concina ◽  
Alberto Vomiero

Molybdenum sulfide (MoS2) has emerged as a promising catalyst for hydrogen evolution applications. The synthesis method mainly employed is a conventional hydrothermal method. This method requires a longer time compared to other methods such as microwave synthesis methods. There is a lack of comparison of the two synthesis methods in terms of crystal morphology and its electrochemical activities. In this work, MoS2 nanosheets are synthesized using both hydrothermal (HT-MoS2) and advanced microwave methods (MW-MoS2), their crystal morphology, and catalytical efficiency towards hydrogen evolution reaction (HER) were compared. MoS2 nanosheet is obtained using microwave-assisted synthesis in a very short time (30 min) compared to the 24 h hydrothermal synthesis method. Both methods produce thin and aggregated nanosheets. However, the nanosheets synthesized by the microwave method have a less crumpled structure and smoother edges compared to the hydrothermal method. The as-prepared nanosheets are tested and used as a catalyst for hydrogen evolution results in nearly similar electrocatalytic performance. Experimental results showed that: HT-MoS2 displays a current density of 10 mA/cm2 at overpotential (−280 mV) compared to MW-MoS2 which requires −320 mV to produce a similar current density, suggesting that the HT-MoS2 more active towards hydrogen evolutions reaction.


2010 ◽  
Vol 203 (2) ◽  
pp. 415-418 ◽  
Author(s):  
Kushal D. Bhatte ◽  
Pawan Tambade ◽  
Shin-ichiro Fujita ◽  
Masahiko Arai ◽  
Bhalchandra M. Bhanage

RSC Advances ◽  
2015 ◽  
Vol 5 (44) ◽  
pp. 34761-34768 ◽  
Author(s):  
B. Nageswara Rao ◽  
P. Ramesh Kumar ◽  
O. Padmaraj ◽  
M. Venkateswarlu ◽  
N. Satyanarayana

Porous α-Fe2O3 nanostructures were developed in the presence of a base catalyst by a rapid microwave assisted hydrothermal method.


2014 ◽  
Vol 17 (4) ◽  
pp. 933-939 ◽  
Author(s):  
Fabiana Villela da Motta ◽  
Ana Paula de Azevedo Marques ◽  
Vinícius Dantas de Araújo ◽  
Mara Tatiane de Souza Tavares ◽  
Mauricio Roberto Bomio Delmonte ◽  
...  

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