scholarly journals Erratum to “Preparation of certified reference materials for cotton fabric’s dye transfer inhibition performance test of household washing machines”

2020 ◽  
Vol 15 ◽  
pp. 155892502095887
2020 ◽  
Vol 15 ◽  
pp. 155892502094116 ◽  
Author(s):  
Mingqi Guo ◽  
Yun He ◽  
Li Jiang ◽  
Qingbo Yang ◽  
Jianli Liu ◽  
...  

At present, many well-known brands of washing machines in the market are equipped with dye transfer inhibition washing procedures. However, there is no standardized sample available for the evaluation of the dye transfer inhibition washing procedure, and there is no comparability and access standard of the high-quality washing machine with the related functions. In this article, the certified reference materials for the evaluation of the dye transfer inhibition function will be prepared, which consist of certified reference material of white cotton fabric and that of dyed cotton fabric. The certified reference material of white fabric is made of bleached plain fabric, and that of dyed fabric is made with different reactive red dyes and dyeing processes. The size and manufacturing process of the whole set of standardized samples for the evaluation of dye transfer inhibition are selected and determined through experiments. The preparation of the standardized sample for the evaluation of dye transfer inhibition will improve the research and design of the functional washing procedure, which can better solve the pain point when dark and light clothes are washed together.


2020 ◽  
Vol 7 (1) ◽  
Author(s):  
Mingqi Guo ◽  
Li Jiang ◽  
Qingbo Yang ◽  
Chang Sun ◽  
Jianli Liu ◽  
...  

AbstractIn order to prevent light-colored clothes from being stained by dyes released from dark clothes during the washing process, some new-type washing machines have developed the dye transfer inhibition washing program. However, there is no certified reference materials for the test of dye transfer inhibition function. To this end, cotton fabric and reactive dyes are used as experimental materials to prepare standardized samples to evaluate the dye transfer inhibition function of washing machines. Firstly, the single factor analysis method is used to analyze the significance of the dyeing parameters including dye dosage, dyeing temperature, sodium sulfate dosage and sodium carbonate dosage. Secondly, a 4-factor 5-level experimental design and theoretical prediction of the best dyeing parameters are successively carried out through central composite design and response surface method. Two evaluation indicators, the dye release amount of the standardized sample of dyed fabric and the color difference value of the standardized sample of white fabric after washing, are proposed as the response values for response surface analysis to search the optimal dying parameters in theory. The optimal dyeing parameters obtained through response surface analysis are that the dosage of dye is 5.63% (owf), the dyeing temperature is 60 °C, the dosage of sodium sulfate is 93.60 g/L, and the dosage of sodium carbonate is 15 g/L. Experimental results indicate that the standardized samples prepared with optimal dyeing parameters can effectively distinguish the dye transfer inhibition function of washing machines.


2020 ◽  
pp. 66-72
Author(s):  
Irina A. Piterskikh ◽  
Svetlana V. Vikhrova ◽  
Nina G. Kovaleva ◽  
Tatyana O. Barynskaya

Certified reference materials (CRM) composed of propyl (11383-2019) and isopropyl (11384-2019) alcohols solutions were created for validation of measurement procedures and control of measurement errors of measurement results of mass concentrations of toxic substances (alcohol) in biological objects (urine, blood) and water. Two ways of establishing the value of the certified characteristic – mass consentration of propanol-1 or propanol-2 have been studied. The results obtained by the preparation procedure and comparison with the standard are the same within the margin of error.


2017 ◽  
Vol 13 (7) ◽  
pp. P1512
Author(s):  
Sébastien Boulo ◽  
Julia Kuhlmann ◽  
Andreas Leinenbach ◽  
Tobias Bittner ◽  
Leentje Demeyer ◽  
...  

Author(s):  
Juliane Riedel ◽  
Sebastian Recknagel ◽  
Diana Sassenroth ◽  
Tatjana Mauch ◽  
Sabine Buttler ◽  
...  

AbstractZearalenone (ZEN), an estrogenic mycotoxin produced by several species of Fusarium fungi, is a common contaminant of cereal-based food worldwide. Due to frequent occurrences associated with high levels of ZEN, maize oil is a particular source of exposure. Although a European maximum level for ZEN in maize oil exists according to Commission Regulation (EC) No. 1126/2007 along with a newly developed international standard method for analysis, certified reference materials (CRM) are still not available. To overcome this lack, the first CRM for the determination of ZEN in contaminated maize germ oil (ERM®-BC715) was developed in the frame of a European Reference Materials (ERM®) project according to the requirements of ISO Guide 35. The whole process of CRM development including preparation, homogeneity and stability studies, and value assignment is presented. The assignment of the certified mass fraction was based upon an in-house study using high-performance liquid chromatography isotope dilution tandem mass spectrometry. Simultaneously, to support the in-house certification study, an interlaboratory comparison study was conducted with 13 expert laboratories using different analytical methods. The certified mass fraction and expanded uncertainty (k = 2) of ERM®-BC715 (362 ± 22) μg kg−1 ZEN are traceable to the SI. This reference material is intended for analytical quality control and contributes to the improvement of consumer protection and food safety. Graphical abstract


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