Solid State Structure and Absolute Configuration of Filifolinol Acetate
2011 ◽
Vol 6
(6)
◽
pp. 1934578X1100600
Keyword(s):
X Ray
◽
Careful reevaluation of the 1H and 13C NMR spectroscopic data of filifolinol acetate (4) led to the reassignment of the C-10 and C-11 signals, as well as the gem-dimethyl signals. Single crystal X-ray analysis provided an independent structural confirmation of 4, and comparison of the experimental vibrational circular dichroism spectrum with calculations performed using density functional theory provided the absolute configuration of this 3H-spiro-1-benzofuran-2,1′-cyclohexane and related molecules.
2015 ◽
Vol 10
(8)
◽
pp. 1934578X1501000
2010 ◽
Vol 75
(7)
◽
pp. 2179-2188
◽
1998 ◽
Vol 120
(44)
◽
pp. 11323-11334
◽
2007 ◽
Vol 119
(1-3)
◽
pp. 19-28
◽
2009 ◽
Vol 113
(46)
◽
pp. 13013-13022
◽
Keyword(s):