Sintering studies of synthesised manganese-oxide-doped calcium phosphate via wet chemical precipitation method

2014 ◽  
Vol 18 (sup6) ◽  
pp. S6-147-S6-150
Author(s):  
A. Norakmal ◽  
S. Ramesh ◽  
C. Y. Tan ◽  
A. Muchtar ◽  
B. K. Yap ◽  
...  
RSC Advances ◽  
2014 ◽  
Vol 4 (40) ◽  
pp. 20902-20908 ◽  
Author(s):  
Reza Zamiri ◽  
Avito Rebelo ◽  
Golriz Zamiri ◽  
Atena Adnani ◽  
Ajay Kuashal ◽  
...  

We report on the synthesis of ZnO nanoplates and ZnO nanoplate/Ag nanoparticle heterostructures via a simple and cost effective wet chemical precipitation method.


2021 ◽  
pp. 132142
Author(s):  
Mashrafi Bin Mobarak ◽  
Md. Sahadat Hossain ◽  
Zenefar Yeasmin ◽  
Monika Mahmud ◽  
Md. Maksudur Rahmana Sazia Sultana ◽  
...  

2014 ◽  
Vol 970 ◽  
pp. 20-25 ◽  
Author(s):  
Ahmad Nawawi Natasha ◽  
Ramesh Singh ◽  
Mohd Hamdi Bin Abd Shukor ◽  
Tan Chou Young ◽  
Judha Purbolaksono ◽  
...  

Hydroxapatite (HA) is a stable phase with low dissolution rate in body fluid. Meanwhile, β-tricalcium phosphate (β-TCP) is rather soluble but the dissolution rate is too fast for bone bonding. Therefore a mixture of both is desirable to control the bioresorbability. In this work, calcium phosphate powder has been synthesized via sol gel and wet precipitation method to compare phase behaviour of these powders upon calcination. XRD result clearly revealed that both as-synthesized powders were pure HA with good purity. The decomposition of HA to TCP took place in the range of 700-800 °C and 800-900 °C for sol gel and wet chemical precipitation powder, respectively. The weight loss detected at 700-850°C in TGA analysis confirmed the presence of this biphasic mixtures.From FTIR analysis, profound change in OH-band intensity was attributed to the increased in HA crystallinity with calcination temperature.


RSC Advances ◽  
2019 ◽  
Vol 9 (29) ◽  
pp. 16541-16553
Author(s):  
R. Thangarasu ◽  
B. Babu ◽  
N. Senthil Kumar ◽  
Mon-Shu Ho ◽  
O. N. Balasundaram ◽  
...  

A wet chemical precipitation method was used to synthesize pure and Cu-doped (3, 5 or 7 at%) V2O5 nanorods and photodiodes were fabricated.


2013 ◽  
Vol 12 (05) ◽  
pp. 1350036 ◽  
Author(s):  
KIBRIYA SIDDIQUE ◽  
BHABESH KUMAR NATH ◽  
SANJIB KARMAKAR

We report the synthesis of copper oxide ( CuO ) nanoparticles prepared by wet chemical precipitation method. The structural and dielectric properties are studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and complex impedance spectroscopy as a function of frequencies from 40 KHz to 100 KHz in the range of temperatures (308–393K). Maximum value of dielectric constants are found to be in the order of 106 which increases with increase in temperatures. From XRD data it is found that the particle size increases with increase in calcination temperatures. SEM with energy dispersive X-ray fluorescence spectrometer (EDX) results show that only CuO is present in the prepared sample. The selected area electron diffraction (SAED) pattern by TEM shows that uniform size distributions of CuO nanoparticles are present in the sample.


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