Corrosion fatigue crack growth rates of X70 base metal and heat affected zone in H2S corrosive environment

2014 ◽  
Vol 50 (1) ◽  
pp. 18-25 ◽  
Author(s):  
J. Wang ◽  
X. Y. Li ◽  
Y. L. Zhang ◽  
W. Miao ◽  
S. R. Li
Author(s):  
Takeshi Ogawa ◽  
Yuki Sugiyama ◽  
Toshihiko Kanezaki ◽  
Noboru Hayashi

A hydrogen gas container is one of the critical components for fuel cell vehicles (FCV), which is expected for CO2-free personal transportation. In the early stage of commercial FCV, the major container structure will be a compressed hydrogen gas cylinder, which consists of metal or plastic linear with metal boss and carbon fiber reinforced plastics (CFRP). In order to choose an appropriate material for the metal boss and metal liner, corrosion resistance should be evaluated for various aspects such as corrosion fatigue crack growth (CFCG) and stress corrosion cracking (SCC) in the high pressure hydrogen as well as in salt water environment for the purpose of vehicle use. In the present study, CFCG characteristics were evaluated for several aluminum alloys in air and in salt waters with various concentrations. The results showed that the crack growth rates were accelerated in salt water for all the materials and their environmental sensitivities were compared. The concentrations of the salt water exhibited minor effect on the fatigue crack growth rates. These CFCG characteristics were compared with the corrosion test results based on the ISO 7866 Annex A [1]. A basic idea was proposed for the evaluation of compressed hydrogen gas containers and the important material properties were suggested.


Author(s):  
Stephen J. Hudak ◽  
James H. Feiger ◽  
Jason A. Patton

Corrosion-fatigue is a significant design consideration in deepwater floating production systems. Mechanical loading is accentuated due to the compliant nature of these structures, and sour service conditions can also occur either due to the nature of the crude production or due to seawater flooding of the reservoir to enhance production yield. New high-strength riser steels have recently been developed to meet the demands of deepwater development. The objective of this study was to characterize the corrosion-fatigue resistance of these materials in terms of crack growth rates as a function of applied stress intensity factor range (ΔK), as well as cyclic loading frequency. Experiments were performed on five different steels with yield strengths ranging from 848 to 1080 MPa. Two environments were considered: seawater with cathodic protection to simulate the environment outside of the riser, and a sour brine environment with low oxygen (< 10 ppb) to simulate the environment inside the riser. Not all steels were tested in the sour brine environment since not all were designed to operate in sour service. For both environments, higher strength steels were found to exhibit higher growth rates and lower saturation frequencies. Fatigue crack growth rates as a function of ΔK were also measured, and exhibited two different frequency responses. At high ΔK, the classical frequency response occurred: decreased frequency gave increased crack growth rates. At low ΔK, an inverse frequency effect was observed: deceased frequency gave decreased crack growth rates, as well as increased corrosion-fatigue crack growth thresholds. These differences are believed to be caused by different underlying processes controlling crack growth — specifically, material-environment reaction kinetics at high ΔK, and crack closure due to corrosion-product wedging at low ΔK. The practical significance of these results is discussed, including selection of frequencies for corrosion-fatigue crack growth testing, and applicability of results to structural integrity assessments.


2009 ◽  
Vol 65 ◽  
pp. 9-18 ◽  
Author(s):  
D. Angeles Herrera ◽  
J.L. González Velázquez

The fatigue crack growth of longitudinal SAW welds of a API 5L X42 steel pipe was evaluated using curved three point bend test specimens, where the radius of curvature of the specimens was equal to the pipe radius, so that no extensive machining or flattening was required. The fatigue crack growth tests were done in a servohydraulic closed loop machine under load control, in air at room temperature. The da/dN vs ∆K plots and Paris’s equation constants were obtained for the base metal, deposited metal and heat affected zone in the CR orientation, which corresponds to the short transverse direction of the pipe. The greater resistance to fatigue crack growth was the base metal, whereas the deposited metal showed the least resistance to the fatigue crack propagation. The deposited metal and the heat affected zone behaved according to Paris’s law, unlike the base metal, that showed a high dispersion of the fatigue crack growth rates. This behavior was due to the propagation of the crack in the direction transverse to the banded microstructure. Furthermore, the differences in fatigue crack growth rates among each zone were also related to the roughness of the fracture surfaces and fracture toughness.


Author(s):  
Mohammad Hassan Marvasti ◽  
Weixing Chen ◽  
Richard Kania ◽  
Robert Worthingham ◽  
Greg Van Boven

Corrosion fatigue and fatigue crack growth in air tests were comparatively conducted on an X52 pipelines steel. Fatigue crack growth rates in air were lower than corrosion fatigue crack growth rates due to the absence of hydrogen and mechanical dormancy arisen from low temperature creep at low cyclic frequencies. Mechanical dormancy can commonly occur during operation of both oil and gas pipelines. Crack growth in near neutral pH environments can be well rationalized by a combined loading factor, (ΔK)2Kmax/fα, which reflects the synergistic interaction between the mechanical driving force and the hydrogen effects. Hydrogen plays a decisive role in terms of crack growth in pipelines steels exposed to near neutral pH environments.


Author(s):  
Stephen J. Hudak ◽  
Guadalupe B. Robledo ◽  
James H. Feiger

Corrosion-fatigue is a significant design consideration in deepwater floating production systems. Mechanical loading is accentuated due to the compliant nature of these structures, and sour service conditions can also occur either due to the nature of the crude production or due to seawater flooding of the reservoir to enhance production yield. Consequently, over the past ten years a significant amount of corrosion-fatigue data have been generated on the influence of sour brine environments on conventional steels (X 65 and X 70), and more recently, on new higher strength steels specifically developed for deepwater applications. Although corrosion-fatigue data have also been generated for Ti-alloys in seawater, little or no data are available for Ti alloys in sour brine environment. The goal of this study, sponsored by the US DOE through the RPSEA Project, was to fill this knowledge gap by generating corrosion-fatigue data on a Ti Grade 29 alloy in sour brine with low-oxygen representative of the environment inside risers and stress joints. Corrosion-fatigue crack growth rates were initially obtained at a constant crack-tip driving force, ΔK, to assess the influence of cyclic loading frequency. These results were used to determine optimum frequencies for subsequent fatigue crack growth rate testing as a function of ΔK, thereby providing results that can be used in engineering critical assessments to establish NDE inspection limits. In addition, classical corrosion fatigue S-N fatigue data, which are typically utilized in fatigue design, were also generated on Ti-29 using full-thickness strip fatigue specimens extracted from the pipe wall. All data were generated on base material. The Ti-29 data are also compared to those from a companion study on high strength steels. At high ΔK, the baseline air fatigue crack growth rates in Ti-29 exhibited rates that were 3X-4X greater than those in the steels due to the effect of the lower modulus and lower ductility in Ti-29 compared to those in the steels. In contrast, at low ΔK, the rates in Ti-29 in air were equal to or less than those in the steels of comparable strength levels. In sour brine at ΔK values of 20 MPa√m and above, the rates in sour brine were up to 2X-4X greater than those in air; however, at low ΔK the rates in sour brine merged with those in air. Consequently, at high ΔK, the higher baseline rates in air plus the increase of 2X-4X in the sour brine environment resulted in corrosion-fatigue crack growth rates in Ti-29 that approached those of the steels. However, at low ΔK in sour brine, a reduction in the local crack driving force in Ti-29, believed to be due to roughness-induced crack closure, resulted in Ti-29 rates that were comparable to the air crack growth rates in steels. The S-N fatigue lives of Ti-29 in sour brine were reduced by a factor of about 2X or less compared to those in air. These S-N fatigue lives in sour brine were 8X-10X better than those in the steels in the sour brine. Thus, for sour-service applications in the intermediate- and high-cycle fatigue regimes, Ti-29 has significantly better sour corrosion fatigue performance than that of steels with comparable strength levels.


Sign in / Sign up

Export Citation Format

Share Document