scholarly journals Effects of Molecular Mobility on High Resolution Solid State NMR Spectra —Model Systems—

2020 ◽  
pp. 167-187
Author(s):  
William L. Earl
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Molecular Mobility ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Model Systems

13C high resolution solid state NMR spectra of Chinese coals

1997 ◽  
Vol 40 (1) ◽  
pp. 65-72
Author(s):  
Deyu Chen ◽  
Jianzhi Hu ◽  
Chaohui Ye
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Nmr Spectra

scholarly journals A Sedimented Sample of a 59 kDa Dodecameric Helicase Yields High-Resolution Solid-State NMR Spectra

2012 ◽  
Vol 51 (31) ◽  
pp. 7855-7858 ◽  
Author(s):  
Carole Gardiennet ◽  
Anne K. Schütz ◽  
Andreas Hunkeler ◽  
Britta Kunert ◽  
Laurent Terradot ◽  
...  
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Nmr Spectra

Obtaining accurate chemical shifts for all magnetic nuclei (1H, 13C, 17O, and 27Al) in tris(2,4-pentanedionato-O,O′)aluminium(III) — A solid-state NMR case study

2011 ◽  
Vol 89 (9) ◽  
pp. 1087-1094 ◽  
Author(s):  
Alan Wong ◽  
Mark E. Smith ◽  
Victor Terskikh ◽  
Gang Wu
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Chemical Shifts ◽  
Dft Method ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Multiple Quantum ◽  
Isotropic Chemical Shifts

We report a complete set of high-resolution solid-state NMR spectra for all magnetic nuclei (1H, 13C, 17O, and 27Al) in the α-form of tris(2,4-pentanedionato-O,O′)aluminium(III), α-Al(acac)3. These high-resolution NMR spectra were obtained by using a host of solid-state NMR techniques: standard cross-polarization under the magic-angle spinning (CPMAS) method for 13C, 1-D homonuclear decoupling using the windowed DUMBO sequence for 1H, double-rotation (DOR) for 17O and 27Al, and multiple-quantum MAS for 27Al. Some experiments were performed at multiple magnetic fields. We show that the isotropic chemical shifts obtained for 1H, 13C, 17O, and 27Al nuclei in α-Al(acac)3 are highly resolved and accurate, regardless of the nature of the targeted nuclear spins (i.e., spin-1/2 or quadrupolar) and, as such, can be treated equally in comparison with computational chemical shifts obtained from a gauge-including projector-augmented wave (GIPAW) plane-wave pseudopotential DFT method.

scholarly journals NMR crystallography: The effect of deuteration on high resolution 13C solid state NMR spectra of a 7-TM protein

2007 ◽  
Vol 1768 (12) ◽  
pp. 3029-3035 ◽  
Author(s):  
K. Varga ◽  
L. Aslimovska ◽  
I. Parrot ◽  
M.-T. Dauvergne ◽  
M. Haertlein ◽  
...  
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Nmr Crystallography

High-resolution solid-state NMR of carbon bonded to deuterium

1987 ◽  
Vol 73 (2) ◽  
pp. 239-243 ◽  
Author(s):  
Scott D Swanson ◽  
S Ganapathy ◽  
Robert G Bryant
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr
Sign in / Sign up

Export Citation Format

Share Document