Studies on the Reactions between Oxides in Solid State at Higher Temperatures. II. The Reaction between Calcium Oxide and Titanium Oxide and the Photo-sensitivity of Calcium Titanate

Some recent progress in solid state 47,49Ti NMR is described and reviewed. The metallic-state work described covers metals such as hep titanium, TiB2 , a number of intermetallics such as TiAl2 and TiAl3· The inorganic work covers the various titanium oxide based materials including the TiO2 polymorphs, anatase, rutile and brookite. The gel work covers the evolution of crystalline titania from gels formed by hydrolysis of titanium isopropoxide. Some complementary data from 17O and 13C NMR and powder X-ray diffraction is also included.

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Structure and Electrochemical Performance of Niobium-Substituted Spinel Lithium Titanium Oxide Synthesized by Solid-State Method

Journal of The Electrochemical Society ◽

10.1149/1.3533391 ◽

2011 ◽

Vol 158 (3) ◽

pp. A266 ◽

Cited By ~ 73

Author(s):

Ting-Feng Yi ◽

Ying Xie ◽

J. Shu ◽

Zhenhong Wang ◽

Cai-Bo Yue ◽

...

Keyword(s):

Solid State ◽

Electrochemical Performance ◽

Titanium Oxide ◽

Solid State Method ◽

Lithium Titanium Oxide ◽

State Method ◽

Lithium Titanium

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New concept of an all-solid-state reference electrode using a film of lithium lanthanum titanium oxide (LLTO)

Electrochimica Acta ◽

10.1016/j.electacta.2012.07.051 ◽

2012 ◽

Vol 80 ◽

pp. 418-425 ◽

Cited By ~ 8

Author(s):

Stéphanie Lorant ◽

Claude Bohnke ◽

Michaël Roffat ◽

Odile Bohnke

Keyword(s):

Solid State ◽

Titanium Oxide ◽

Reference Electrode ◽

State Reference

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Role of an intermediate phase in solid state reaction of hydrous titanium oxide with potassium carbonate

Materials Chemistry and Physics ◽

10.1016/j.matchemphys.2005.05.022 ◽

2005 ◽

Vol 94 (2-3) ◽

pp. 401-407 ◽

Cited By ~ 27

Author(s):

Chang Liu ◽

Xiaohua Lu ◽

Gang Yu ◽

Xin Feng ◽

Qitu Zhang ◽

...

Keyword(s):

Solid State ◽

Titanium Oxide ◽

Potassium Carbonate ◽

Solid State Reaction ◽

Intermediate Phase

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Lithium titanium oxide synthesis by solid-state reaction for lithium adsorption from artificial brine source

IOP Conference Series Earth and Environmental Science ◽

10.1088/1755-1315/882/1/012005 ◽

2021 ◽

Vol 882 (1) ◽

pp. 012005

Author(s):

I W C W H Tangkas ◽

W Astuti ◽

Sutijan ◽

S Sumardi ◽

H T B M Petrus

Keyword(s):

Solid State ◽

Titanium Oxide ◽

Solid State Reaction ◽

Crystal Size ◽

Supply And Demand ◽

Lithium Ion ◽

Alternative Source ◽

Solid Ratio ◽

Lithium Titanium Oxide ◽

Lithium Titanium

Abstract Lithium and titanium are the materials that have an essential role in today’s industrial world, especially in LIBs (lithium-ion batteries). LIBs have become an important issue nowadays due to the imbalance between supply and demand. Lithium adsorption from brine sources becomes an alternative source using various methods. This study aims to find the characteristic of LTO (lithium titanium oxide), which was synthesized by the solid-state reaction process for adsorption lithium from an artificial brine source. The variables studied were temperature and the solid-solid ratio of Li and Ti. Each LTO obtained was analyzed using XRD to define the crystal structure and composition of LTO formed. The LTO product has a monoclinic structure, with more significant peaks in 2-theta 18° and 43°. The size of crystals formed is influenced by temperature and ratio of solid Li/Ti. The largest crystal formed at a temperature of 600°C and 750°C is 512 nm and 50 nm. The higher the temperature, the smaller the crystal sized formed and the higher Li/Ti solid ratio, the greater the crystal size formed.

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