scholarly journals SEM Observation at High Magnification and EDX Analysis of Insulating Sample by Diluted Ionic Liquid

Hyomen Kagaku ◽  
2011 ◽  
Vol 32 (10) ◽  
pp. 659-663 ◽  
Author(s):  
Long ZE ◽  
Susumu IMASHUKU ◽  
Masahiro ICHIDA ◽  
Jun KAWAI
Keyword(s):  
Ionic Liquid ◽  
High Magnification ◽  
Edx Analysis ◽  
Sem Observation

scholarly journals New Preparation Method using Ionic Liquid for Fast and Reliable SEM Observation of Biological Specimens

2014 ◽  
Vol 20 (S3) ◽  
pp. 1012-1013 ◽  
Author(s):  
Mari Sakaue ◽  
Masamichi Shiono ◽  
Mami Konomi ◽  
Junichiro Tomizawa ◽  
Eiko Nakazawa ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Preparation Method ◽  
Sem Observation

scholarly journals SEM Observation of Wet Lily Pollen Grains Pretreated with Ionic Liquid

2014 ◽  
Vol 83 (4) ◽  
pp. 317-321 ◽  
Author(s):  
Fuminori Komai ◽  
Kanako Okada ◽  
Yuko Inoue ◽  
Mitsunori Yada ◽  
Osamu Tanaka ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Pollen Grains ◽  
Sem Observation ◽  
Lily Pollen

scholarly journals Possibility of Scanning Electron Microscope Observation and Energy Dispersive X-Ray Analysis in Microscale Region of Insulating Samples Using Diluted Ionic Liquid

2012 ◽  
Vol 18 (2) ◽  
pp. 365-370 ◽  
Author(s):  
Susumu Imashuku ◽  
Tetsuo Kawakami ◽  
Long Ze ◽  
Jun Kawai
Keyword(s):  
Ionic Liquid ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Energy Dispersive ◽  
Light Elements ◽  
Standard Samples ◽  
X Ray ◽  
Spectrometry Analysis ◽  
Sem Observation ◽  
Scanning Electron

AbstractThe possibility of scanning electron microscope (SEM) observation and energy dispersive X-ray (EDX) spectrometry analysis in microscale regions of insulating samples using diluted ionic liquid was investigated. It is possible to obtain clear secondary electron images of insulating samples such as a rock and mineral at 5,000 times magnification by dropping 10 μL of 1 wt% of 1-ethyl-3-methylimidazolium acetate (EMI-CH3COO) diluted with ethanol onto the samples. We also obtained EDX spectra of the samples in microscale regions (∼5 μm2) without overlapping EDX spectra of other minerals with different composition. It might be possible to perform quantitative analysis of the samples if a method that does not need standard samples is applied or an X-ray detector sensitive for light elements was attached. The method of dropping 1 wt% EMI-CH3COO diluted with ethanol onto insulating samples is useful for SEM observation, EDX analysis in microscale regions, and the preservation of scarce rock and mineral samples because ionic liquid can be easily removed with acetone.

FE-SEM observation of swelled seaweed using hydrophilic ionic liquid; 1-butyl-3-methylimidazolium tetrafluoroborate

2012 ◽  
Vol 76 (1) ◽  
pp. 66-71 ◽  
Author(s):  
Chisato Takahashi ◽  
Takashi Shirai ◽  
Masayoshi Fuji
Keyword(s):  
Ionic Liquid ◽  
Sem Observation

The Properties of Refined Glasses with Aluminum Hydroxide Nano-Molecules

2015 ◽  
Vol 227 ◽  
pp. 47-50
Author(s):  
Marcin Drajewicz ◽  
Maciej Pytel ◽  
Paweł Rokicki ◽  
Marek Góral
Keyword(s):  
Aluminum Hydroxide ◽  
Glass Surface ◽  
Inorganic Compounds ◽  
Surface Layers ◽  
Edx Analysis ◽  
Sem Observation ◽  
Calcium Silicon ◽  
Glass Surfaces ◽  
Glass Properties

New refining technology of soda – calcium – silicon glass surfaces with inorganic compounds nanomolecules has been presented in the study. In order to determine modification of the glass surface SEM observation and EDX analysis have been carried out. The glass samples were subjected to the UV-VIS, photo-elasticity and ellipsometry examinations. From obtained results follows, that refining of the glass surface by nanopowder aluminum hydroxide compounds provides forming of very thin surface layers. This type of modification improves physical glass properties. As the example results of microhardness refined glass are presented in the article.Keywords: glass, surface, nanoparticles, refining

SEM Observation of Wet Biological Specimens Pretreated with Room-Temperature Ionic Liquid

ChemBioChem ◽  
2011 ◽  
Vol 12 (17) ◽  
pp. 2547-2550 ◽  
Author(s):  
Tetsuya Tsuda ◽  
Noriko Nemoto ◽  
Koshi Kawakami ◽  
Eiko Mochizuki ◽  
Shoko Kishida ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Room Temperature ◽  
Room Temperature Ionic Liquid ◽  
Sem Observation

scholarly journals SEM-EDX Analysis of Insulator Specimens by Diluted Ionic Liquid ^|^mdash; Application to Volcanic Particles ^|^mdash;

2012 ◽  
Vol 61 (11) ◽  
pp. 947-951
Author(s):  
Long ZE ◽  
Susumu IMASHUKU ◽  
Jun KAWAI ◽  
Daisuke MIKI ◽  
Susumu TOHNO
Keyword(s):  
Ionic Liquid ◽  
Edx Analysis

[Te8][NbOCl4]2containing an infinite chain-like {[Te–Te–Te–(Te5)]2+}npolycation

2012 ◽  
Vol 68 (10) ◽  
pp. i68-i70 ◽  
Author(s):  
Claus Feldmann ◽  
Dominic Freudenmann
Keyword(s):  
Ionic Liquid ◽  
Single Crystals ◽  
Structure Analysis ◽  
Title Compound ◽  
Energy Dispersive ◽  
The Novel ◽  
X Ray Diffraction ◽  
X Ray ◽  
Edx Analysis ◽  
Lattice Symmetry

The title compound, [Te8][NbOCl4]2, was obtained as translucent black crystals by reaction of elemental tellurium, niobium(V) chloride and niobium(V) oxychloride in the ionic liquid BMImCl (BMImCl is 1-butyl-3-methylimidazolium chloride). The synthesis was performed in argon-filled glass ampoules. According to X-ray structure analysis based on single crystals, the title compound crystallizes with triclinic lattice symmetry and consists of infinite {[Te8]2+}ncations associated with pyramidal [NbOCl4]−anions. The novelcatena-octatellurium(2+) cation is composed of Te5rings that are linkedviaTe3units [Te—Te = 2.6455 (18)–2.8164 (19) Å]. The composition and purity of [Te8][NbOCl4]2were further confirmed by energy-dispersive X-ray diffraction (EDX) analysis.

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