Surface characteristics of oxide films on titanium alloys formed by AC-type microarc oxidation combined with hydrothermal treatment

2007 ◽  
Vol 280-283 ◽  
pp. 1537-1540
Author(s):  
Fu Liu ◽  
Fu Ping Wang ◽  
Tadao Shimizu ◽  
K. Igarashi ◽  
Lian Cheng Zhao

An oxide film containing Ca and P was obtained in an electrolyte containing calcium glycerphosphate (Ca-GP) and calcium acetate (CA) by microarc oxidation. The surfaces of the oxide films were porous and rough, and the Ca/P ratio in the oxide film was 1.71 when the oxide film was formed in the electrolyte containing 0.06 M Ca-GP and 0.25 M CA at current density 50 A/m2 and final voltage 350 V. The oxide film with Ca/P ration 1.71 was treated hydrothermally at 190°C for 10 hours in an autoclave. It was found that hydroxyapatite crystals were precipitated on the oxide film after hydrothermal treatment. The oxide films were investigated by means of electron probe micro analyzer, X-ray diffraction, scanning electron microcopy before and after hydrothermal treatment.


Author(s):  
G.M. Schueler ◽  
J. Engmann ◽  
T. Marx ◽  
R. Haberland ◽  
J.C. Aurich

2017 ◽  
Vol 264 ◽  
pp. 66-69
Author(s):  
Fadilah Darus ◽  
Mariatti Jaafar

Carbonate apatite would be ideal for bone substitute due to its composition of 4-8% carbonate similar to bone mineral. The purpose of the present study was to produce carbonate apatite scaffold by using hydrothermal treatment of β-TCP scaffold as a precursor. The effect of different solutions on hydrothermal treatment was studied. The microstructure of scaffold before and after hydrothermal were characterized by scanning electron microscopy (SEM). It is observed that surface characteristics are governed by the types of immersion solution. The typical smooth surface of the β-TCP scaffold was observed before hydrothermal. Different morphology was observed after hydrothermal in different solutions. X-Ray Diffraction (XRD) pattern indicates that the peak of apatite with low intensities present after hydrothermal treatment in sodium hydrogen carbonate solution.


CORROSION ◽  
2000 ◽  
Vol 56 (1) ◽  
pp. 24-31 ◽  
Author(s):  
S. V. Gnedenkov ◽  
P. S. Gordienko ◽  
S. L. Sinebrukhov ◽  
O. A. Khrisanphova ◽  
T. M. Skorobogatova

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