Novel Morphology of Voids in Single-Quasicrystalline Icosahedral Al70.5Pd21.0Mn8.5

1998 ◽  
Vol 53 (8) ◽  
pp. 679-683 ◽  
Author(s):  
Y. Waseda ◽  
S. Suzuki ◽  
K. Urbanb

Abstract This paper deals with the morphology and surface chemistry of faceted voids existing in singlequasicrystalline icosahedral Al70.5Pd21.0Mn8.5. By observation with a scanning electron microscope of surfaces obtained by cleavage of the quasicrystal, the habit planes of the dodecahedral voids were identified. The chemical surface composition of the void surface was determined by Auger electron spectroscopy after cleavage in ultra-high vacuum.

1993 ◽  
Vol 1 (8) ◽  
pp. 5-6
Author(s):  
Anthony D. Buonaquisti

Pressure scales can be extremely confusing to new operators. This is not surprising. To my mind, there are three primary areas of confusion.Firstly, the pressure of gas inside an instrument changes over many orders of magnitude during pumpdown. The change is about 9 orders of magnitude for a traditional Scanning Electron Microscope and about 13 orders of magnitude for an ultra-high vacuum instrument such as a Scanning Auger Microprobe.To give an idea about the scale of change involved in vacuum, consider that the change in going from ambient pressure to that inside a typical ultra high vacuum system is like comparing one meter with the mean radius of the planet Pluto's orbit. The fact is that we don't often get to play with things on that scale. As a consequence, many of us have to keep reminding ourselves that 1 X 10-3 is one thousand times the value of 1 X 10-6 - not twice the value.


2001 ◽  
Vol 9 (1) ◽  
pp. 26-27
Author(s):  
Anthony D. Buonaquisti

Pressure scales can be extremely confusing to new operators. This is not surprising. To my mind, there are three primary areas of confusion.Firstly, the pressure of gas inside an instrument changes over many orders of magnitude during pump-down. The change is about 9 orders of magnitude for a traditional Scanning Electron Microscope and about 13 orders of magnitude for an ultra-high vacuum instrument such as a Scanning Auger Microprobe.


Author(s):  
R. Aihara ◽  
S. Saito ◽  
II. Kohinata ◽  
K. Ogura ◽  
H. Otsuji

A compact type field emission scanning electron microscope (JSM-F15) has recently been developed (Fig. 1). Moreover, due to the simplicity of the electron optical column and the automatically controlled ultra high vacuum system, a good quality and high resolution image can easily be obtained.The electron optical column, which is shown in Fig. 2, comprises a field emission gun, an electromagnetic lens, scanning coils, etc. The gun, which is composed of a field emitter, a wehnelt and an anode, is pre-aligned. The accelerating voltage is 15 kV and the emitter tip, made of tungsten single crystal, has a [310] orientation in the electron optical axis. The wehnelt is biased through a feedback circuit so as to maintain the emission current constant without varying the accelerating voltage.The electron probe current at the specimen surface is about 3 × 10-11 amp and the probe diameter is about 30Å at the working distance of 15 mm.


1992 ◽  
Vol 295 ◽  
Author(s):  
Mikio Takai ◽  
Naoki Yokoi ◽  
Ryou Mimura ◽  
Hiroshi Sawaragi ◽  
Ryuso Aihara

AbstractAn ultra high vacuum (UHV) scanning electron microscope (SEM) combined with a scanning tunneling microscope (STM) has been designed and constructed to solve problems, arising from STM surface imaging and nanofabrication using STM tips, such as difficulty in probe tip location and change in tip shape. The system facilitates to image and/or to modify a wide range of area from submicron down to subnanometer. A ZrO/W thermal emitter in a Schottky mode has been used for an electron gun to obtain a low energy spread with a high angular current density. Minimum beam spot diameters of 6 and 12 nm with currents of 100 pA and 4 nA are estimated by optical property calculation for high resolution (SEM) and high current (fabrication) modes, respectively.


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