Gaschromatographisch-massenspektrometrische Analyse neutraler und saurer Oligosaccharide der Frauenmilch als Trimethylsilyläther / Gas Chromatographic Mass Spectrometric Analysis of Neutral and Acid Oligosaccharides from Human Milk as Their Trimethylsilyl Derivatives
1975 ◽
Vol 30
(7-8)
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pp. 451-459
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Keyword(s):
Abstract Gas chromatography and the 20 eV mass spectra of the human milk oligosaccharides fucosido-galactose, fucosido-lactose, di-fucosido-lactose, 3'-N-acetylneuraminyl-lactose, 6'-N-acetylneuraminyl-lactose and of N-acetyllactosamine as pertrimethylsilyl (TMS) ethers are described. The gas chromatographic separation of the L-fucose containing oligosaccharides was performed on Silicone SE 30. The sialic acid containing sugars were separated on DEXSIL 300. The correlations between oligosaccharide structures and mass spectrometric fragmentation pat terns are discussed.
2009 ◽
Vol 1216
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pp. 6024-6032
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2007 ◽
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pp. 88-101
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1997 ◽
Vol 698
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pp. 1-8
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1971 ◽
Vol 35
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pp. 825-838
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2001 ◽
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pp. 1132-1138
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1992 ◽
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pp. 278-284
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1997 ◽
Vol 791
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pp. 367-370
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Vol 690
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pp. 105-113
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2016 ◽
Vol 32
(3)
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pp. 1439-1451
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