Crystal structure, thermal expansion and elastic properties of triclinic betaine hydrogen ammonium sulfate, ((CH3)3NCH2COOH)NH4SO4

1996 ◽  
Vol 211 (2) ◽  
Author(s):  
S. Haussühl ◽  
J. Schreuer
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
Aqueous Solutions ◽  
Single Crystals ◽  
Ammonium Sulfate ◽  
Elastic Properties ◽  
Structure Analysis ◽  
Optical Quality ◽  
X Ray

AbstractLarge single crystals of optical quality of betaine hydrogen ammonium sulfate have been grown from aqueous solutions. An X-ray structure analysis yielded space group

Crystal structure, thermal expansion and elastic properties of triclinic betaine hydrogen dihydrogen triiodate, ((CH3)3NCH2COOH)H2(IO3)3

1996 ◽  
Vol 211 (12) ◽  
Author(s):  
S. Haussühl ◽  
J. Schreuer
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
Aqueous Solutions ◽  
Single Crystals ◽  
Elastic Properties ◽  
Structure Analysis ◽  
Optical Quality ◽  
Space Group ◽  
X Ray

AbstractLarge single crystals of optical quality of betaine hydrogen dihydrogen iodate have been grown from aqueous solutions. An X-ray structure analysis yields space group

Crystal structure, thermal expansion and dielectric properties of monoclinic ethylenediammonium bis(hydrogensuccinate), H3N(CH2)2NH3(HC4H4O4)2

1994 ◽  
Vol 209 (1) ◽  
Author(s):  
J. Schreuer ◽  
T. Münch
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
Dielectric Properties ◽  
Aqueous Solutions ◽  
Single Crystals ◽  
Structure Analysis ◽  
Optical Quality ◽  
Space Group ◽  
X Ray

AbstractLarge single crystals of optical quality of monoclinic ethylenediammonium bis(hydrogensuccinate) were grown from aqueous solutions. An X-ray structure analysis yielded space group

Crystal structure, dielectric, piezoelectric and elastic properties of (±)-tris(ethylenediamine)cobalt(III) nitrate, (±)–[Co(H2N(CH2)2NH2)3](NO3)3

1998 ◽  
Vol 213 (3) ◽  
Author(s):  
S. Haussühl ◽  
J. Schreuer
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
Single Crystals ◽  
Elastic Properties ◽  
Structure Analysis ◽  
Elastic Constants ◽  
Room Temperature ◽  
Optical Quality ◽  
X Ray

AbstractLarge single crystals of optical quality of (±)-tris(ethylenediamine)cobalt(III) nitrate have been grown from aequeous solutions. An X-ray structure analysis yielded space groupPyroelectric, dieletric, piezoelectric and elastic constants have been determined at room temperature. Additionally, we have studied the coefficients of thermal expansion and the thermoelastic constants in the range between 270 K and 350 K. The structure exhibits a nearly trigonal symmetry around the [unk]

Crystal structure, elastic properties and phase transition of triclinic ammonium hydrogen succinate, NH4HC4H4O4

1993 ◽  
Vol 206 (2) ◽  
Author(s):  
S. Haussühl ◽  
J. Schreuer
Keyword(s):  
Crystal Structure ◽  
Phase Transition ◽  
Aqueous Solutions ◽  
Single Crystals ◽  
Elastic Properties ◽  
Structure Analysis ◽  
Optical Quality ◽  
Space Group ◽  
X Ray ◽  
Ammonium Hydrogen

AbstractLarge optical quality, single crystals of triclinic ammonium hydrogen succinate have been grown from aqueous solutions. An X-ray structure analysis yields space group

Thermal expansion, elastic and thermoelastic properties including crystal structure analyses of K-, Rb- and Cs-nitrilotriacetates

2004 ◽  
Vol 219 (10) ◽  
Author(s):  
Eiken Haussühl ◽  
Siegfried Haussühl ◽  
Ekkehart Tillmanns
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
Aqueous Solutions ◽  
Single Crystals ◽  
Optical Quality ◽  
Thermoelastic Properties ◽  
X Ray

AbstractSingle crystals of the title compounds having optical quality and dimensions up to 60 mm have been grown from aqueous solutions. X-ray crystal structure analyses of K

scholarly journals Growth and Characterization of Epsomite Single Crystals Doped with KCl from low Temperature Aqueous Solutions

1970 ◽  
Vol 33 (1) ◽  
pp. 47-54 ◽  
Author(s):  
S Ferdous ◽  
J Podder
Keyword(s):  
Aqueous Solutions ◽  
Single Crystals ◽  
Optical Quality ◽  
Dielectric Studies ◽  
Slow Cooling ◽  
Large Size ◽  
Isothermal Evaporation ◽  
Academy Of Sciences

Highly transparent and well faceted large size epsomite single crystals have been grown in pure form and doped with KCl from aqueous solutions by slow cooling and isothermal evaporation method. The optical quality of the epsomite improves on doping by KCl. Mass growth rates were found to increase with doping of lower concentrations of KCl and then decreases with the higher concentration of KCl. KCl doped epsomite crystal reveals that structures are slightly distorted due to adsorption of Cl- ion into the crystal lattice. DC conductivity along the growth axis for all of the grown crystals increases with temperature in the range of 25 to 70ºC and also increases with the KCl concentration. Dielectric constant is found to be almost independent of frequency up to range of 106Hz. The dielectric studies show the suitability of these grown crystals for optoelectronic applications. DOI: 10.3329/jbas.v33i1.2949 Journal of Bangladesh Academy of Sciences, Vol. 33, No. 1, 47-54, 2009

scholarly journals A Salt Metathesis Route To Ruthenium Carbene Complex Isomers With Pyridine Dicarboxamide-Derived Chelate Pincer Ligands

2007 ◽  
Vol 62 (6) ◽  
pp. 783-790 ◽  
Author(s):  
Carolin Wallenhorst ◽  
Kirill V. Axenov ◽  
Joseph S. M. Samec ◽  
Roland Fröhlich ◽  
Gerhard Erker
Keyword(s):  
Crystal Structure ◽  
Single Crystals ◽  
Structure Analysis ◽  
Crystal Structure Analysis ◽  
Pincer Ligands ◽  
X Ray Diffraction ◽  
X Ray ◽  
Carbene Complex ◽  
Related Complex

Reaction of the doubly deprotonated pyridine 2,6-dicarboxamido ligand (1) with (PCy3)2Cl2 Ru=CHPh (3a) in THF gave a mixture of (lig)(PCy3)Ru=CHPh isomers (4). The pentane soluble N,N,O-4 isomer was isolated by extraction and characterized by X-ray diffraction. The O,N, O-4 isomer was identified in the residue. Single crystals of the closely related complex (lig)(NHC) Ru=CHPh, O,N,O-5, were obtained from the reaction of 1 with (NHC)(PCy3)Cl2Ru=CHPh (3b) and used for the X-ray crystal structure analysis of the system

Physical properties and phase transitions of bis(guanidinium)zirconium bis(nitrilotriacetate)hydrate, [C(NH2)3]2Zr[N(CH2COO)3]2 · H2O

1997 ◽  
Vol 212 (11) ◽  
Author(s):  
E. Haussühl ◽  
E. Tillmanns
Keyword(s):  
Thermal Expansion ◽  
Phase Transitions ◽  
Physical Properties ◽  
Single Crystals ◽  
Optical Quality ◽  
Refractive Indices ◽  
Strong Anisotropy ◽  
Ultrasonic Methods ◽  
Piezoelectric Constants

AbstractLarge single crystals of optical quality of bis(guanidinium)zirconium bis(nitrilotriacetate)hydrate have been grown from aqueous solutions. Complete elastic, thermoelastic and piezoelastic tensors have been determined by ultrasonic methods. In addition, the tensor of thermal expansion, refractive indices, dielectric and piezoelectric constants have been studied in the range between 210 K and 330 K. Most physical properties investigated show a strong anisotropy. The piezoelectric constant

Crystal structure, elastic properties and ferroelastic phase transition of disodium tetrahydrogen tris(adipate) dihydrate Na2H4(C6H8O43 · 2 H2O

1995 ◽  
Vol 210 (8) ◽  
Author(s):  
L. Wiehl ◽  
X.-Q. Liu ◽  
S. Haussühl
Keyword(s):  
Crystal Structure ◽  
Phase Transition ◽  
Thermal Expansion ◽  
Single Crystals ◽  
Elastic Properties ◽  
Elastic Constants ◽  
Ferroelastic Phase Transition

AbstractElastic constants and thermal expansion were measured using large single crystals of monoclinic Na

Preparation and Crystal Structure Determination of [(C2Η5)4N]2Hg3Cl8

1995 ◽  
Vol 50 (1) ◽  
pp. 66-70 ◽  
Author(s):  
Inge Pabst ◽  
Peter Sondergeld ◽  
Mirjam Czjzek ◽  
Hartmut Fuess
Keyword(s):  
Crystal Structure ◽  
Single Crystals ◽  
Structure Analysis ◽  
Structure Determination ◽  
Title Compound ◽  
Monoclinic Space Group ◽  
Space Group ◽  
Coordination Type ◽  
X Ray

The title compound has been prepared in two different ways: First, by boiling single crystals of [(C2H5)4N]HgCl3 in a mixture of n-hexane/n-octane [4:1] at T = 350 K, and second, in a synthesis from stoichiometric quantities of the components. X-ray structure analysis gave the stoichiometry [(C2H5)4N]2Hg3Cl8, monoclinic, space group P21, a = 7.538(3), b = 19.909(6), c = 10.274(3) Å, β = 95.13(1)°, V = 1535.7(9) A3, Z = 2. The basic [Hg3Cl8]2--units form broken zig-zag chains along [100]. The Hg–Cl distances within the [Hg3Cl8]2- clusters range from 2.315(3) to 2.755(4) Å. This is a new coordination type for halomercurates.

Sign in / Sign up

Export Citation Format

Share Document