Densitometric determination of impurities in pharmaceuticals. Part VIII. Simultaneous determination of fluoxetine and (1RS)-3-methylamino-1-phenylpropan-1-ol,N-methyl-3-phenylpropan-1-amine, and C-1 as drug impurities

2002 ◽  
Vol 15 (1) ◽  
pp. 50-55 ◽  
Author(s):  
Jan Krzek ◽  
Anna Maślanka
1986 ◽  
Vol 35 (8) ◽  
pp. 631-635 ◽  
Author(s):  
Yoshikazu YAMAMOTO ◽  
Takahiro AZUMA ◽  
Yoshinori NISHIMURA ◽  
Kazumasa UEDA

1974 ◽  
Vol 28 (6) ◽  
pp. 564-568 ◽  
Author(s):  
L. S. Dale

A direct carrier distillation procedure for the determination of a wide range of impurities in uranium tetrafluoride is described. The method is based on the use of lead chloride as carrier with yttrium oxide to suppress uranium spectral interference. A deep crater electrode further aids in the reduction of spectral interference. Germanium and cobalt are used as internal standards. The method has been adopted for the simultaneous determination of Ag, l, B, Cd, Cr, Cu, Fe, Mg, Mn, Mo, Na, Ni, Si, Sn, Ti, V, and Zn with detection limits in the range 0.1 to 20 ppm and coefficients of variation ranging from 4 to 15%.


1978 ◽  
Vol 48 ◽  
pp. 287-293 ◽  
Author(s):  
Chr. de Vegt ◽  
E. Ebner ◽  
K. von der Heide

In contrast to the adjustment of single plates a block adjustment is a simultaneous determination of all unknowns associated with many overlapping plates (star positions and plate constants etc. ) by one large adjustment. This plate overlap technique was introduced by Eichhorn and reviewed by Googe et. al. The author now has developed a set of computer programmes which allows the adjustment of any set of contemporaneous overlapping plates. There is in principle no limit for the number of plates, the number of stars, the number of individual plate constants for each plate, and for the overlapping factor.


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