Characterization of superdislocation dissociations in Al66Ti25Cr9 with transmission electron microscopy observations and image simulations

1998 ◽  
Vol 13 (3) ◽  
pp. 610-624 ◽  
Author(s):  
Mukul Kumar ◽  
K. J. Hemker

The nature of dissociated superlattice dislocation cores in Al66Ti25Cr9, deformed at room temperature, has been characterized by weak-beam transmission electron microscopy (TEM) and comparison of experimental images with computer-simulated images. The displacement fields associated with narrowly dissociated APB- and SISF-dissociated ‹110› superdislocations were calculated to account for the asymmetry in dislocation contrast and led to a better understanding of the formation of images. Such calculations are a powerful aid, when coupled with image simulations, in distinguishing the “real” intensity peaks from the supplementary peaks that can be generated under experimental imaging conditions. While both APB- and SISF-dissociated superdislocations were identified, the vast majority of superdislocations were determined to be APB-dissociated. Corrected values of the fault energies (γAPB and γSISF ) have been measured for this alloy. These energies and the observed dissociations are shown to be self-consistent.

Author(s):  
R.M. Allen

Theoretical considerations indicate that the strain-sensitive nature of weak beam transmission electron microscopy warrants application of the technique to problems requiring the resolution of complex microstructures (1). Indeed, weak beam microscopy has already become a valuable tool for observing dislocation dissociation (1), crystalline interfaces (2), and fine precipitate structure (3). In this vein, experiments to determine the possible benefits of employing weak beam microscopy in the examination of heterogeneous nucleation on dislocation lines have been performed on samples of Al-3.87 wt.% Zn-1.79 wt.% Mg. Specimens were solutionized, lightly deformed, and then aged for various times at 150°C prior to observation. Figure 1 is a comparison of a bright field and a weak beam micrograph taken of the same region in a sample aged 18 hrs. The precipitates are the stable η (MgZn2) phase.


Author(s):  
M. M. Tsai ◽  
J. M. Howe

Precipitation of γ-TiH in α-Ti-H alloys involves a hcp → fct lattice transformation with hydrogen as an interstitial diffusing element Results obtained from a previous TEM study have shown that the lengthening rate of γ-TiH is diffusionally controlled at 25°C, and possibly interfacially controlled at temperatures of 50°C and higher. Therefore, it is essential to ascertain the presence or absence of hydrogen atoms at the interface. TEM foils from a 800 ppm wt.% Ti-H alloy were analyzed using high-resolution TEM and image simulations in order to determine the effects of hydrogen on high-resolution images of the α-Ti/γ-TiH interface, and EELS was used to determine the whether the hydnde structure was fully formed up to the interface.


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