Characterization of Nanocavities in Silicon Using Small Angle X-Ray Scattering

2007 ◽  
Vol 994 ◽  
Author(s):  
Myriam Dunmont ◽  
Vanessa Coulet ◽  
Gabrielle Regula ◽  
Françoise Bley
Keyword(s):  
Size Distribution ◽  
Small Angle ◽  
Structural Information ◽  
Cavity Size ◽  
X Ray ◽  
X Ray Scattering ◽  
Transmission Electron ◽  
Si Wafer ◽  
Ray Scattering

AbstractThe techniques of small angle X-ray scattering and transmission electron microscopy are applied to characterize the size distribution of nanocavities in a (111) Si wafer multi-implanted with He+ in the Mev range energy. The comparison between both methods shows that they all give access to the same structural information but small angle X-ray scattering additionally offers the possibility to monitor the cavity size distribution during a thermal treatment. Moreover, providing that the collected data are of good quality, the former method also allows the knowledge of the porosity of the implanted Si wafer.

Ultra Small Angle X-Ray Scattering Characterization of Temperature-Sensitive Ferrogels Prepared Using Magnetic Nanoparticles

2013 ◽  
Vol 1453 ◽  
Author(s):  
Kamlesh J. Suthar ◽  
Muralidhar K. Ghantasala ◽  
Derrick C. Mancini ◽  
Jan Ilavsky
Keyword(s):  
Small Angle ◽  
Quantum Interference ◽  
Solution Temperature ◽  
Temperature Sensitive ◽  
X Ray ◽  
X Ray Scattering ◽  
Transmission Electron ◽  
Hydrogel Particle ◽  
Ray Scattering

ABSTRACTTemperature-sensitive ferrogel prepared using Fe3O4 nanoparticles are characterized under varying temperature conditions. The nanoparticles were distributed in Nisopropylacrylamide (NIPAm) during their polymerization to form hydrogel. Particle distribution and agglomeration characteristics of the prepared ferrogels were investigated using ultra small angle x-ray scattering (USAXS) at various temperatures through the Lower Critical Solution Temperature (LCST). Transmission electron microscopy (TEM) was used to estimate the particle size distribution. The magnetic property was investigated using direct current superconducting quantum interference device (DC-SQUID) under hydrated conditions. The USAXS analysis showed an increase in the volume of particles without changing the agglomeration characteristics as the temperature is increased during the measurements. The ferrogel did not show any sedimentation or particle detachment from the gel under thermal cycling. Details of our results and analysis are presented.

Small angle X-ray scattering study of porosity variation in a styrene-divinylbenzene copolymer

1981 ◽  
Vol 46 (7) ◽  
pp. 1675-1681 ◽  
Author(s):  
Josef Baldrian ◽  
Božena N. Kolarz ◽  
Henrik Galina
Keyword(s):  
Small Angle ◽  
Structural Parameters ◽  
Two Phase ◽  
X Ray ◽  
Porosity Variation ◽  
Swelling Agent ◽  
X Ray Scattering ◽  
Styrene Divinylbenzene ◽  
Ray Scattering

Porosity variations induced by swelling agent exchange were studied in a styrene-divinylbenzene copolymer. Standard methods were used in the characterization of copolymer porosity in the dry state and the results were compared with related structural parameters derived from small angle X-ray scattering (SAXS) measurements as developed for the characterization of two-phase systems. The SAXS method was also used for porosity determination in swollen samples. The differences in the porosity of dry samples were found to be an effect of the drying process, while in the swollen state the sample swells and deswells isotropically.

Nanostructural Characterization of Oleyl Acid Phosphate in Poly-α-olefin Using Small-angle X-ray Scattering

2020 ◽  
Vol 49 (7) ◽  
pp. 823-825
Author(s):  
Yojiro Oba ◽  
Ryuhei Motokawa ◽  
Masahiro Hino ◽  
Nozomu Adachi ◽  
Yoshikazu Todaka ◽  
...  
Keyword(s):  
Small Angle ◽  
Acid Phosphate ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

scholarly journals Alpha helical surfactant-like peptides self-assemble into pH-dependent nanostructures

Soft Matter ◽  
2021 ◽  
Vol 17 (11) ◽  
pp. 3096-3104
Author(s):  
Valeria Castelletto ◽  
Jani Seitsonen ◽  
Janne Ruokolainen ◽  
Ian W. Hamley
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Small Angle ◽  
Self Assembly ◽  
X Ray ◽  
Cryogenic Transmission Electron Microscopy ◽  
X Ray Scattering ◽  
Transmission Electron ◽  
Ph Dependent ◽  
Ray Scattering

A designed surfactant-like peptide is shown, using a combination of cryogenic-transmission electron microscopy and small-angle X-ray scattering, to have remarkable pH-dependent self-assembly properties.

scholarly journals Precise and nondestructive characterization of a ‘buried’ nanostructure in a polymer thin film using synchrotron radiation ultra-small angle X-ray scattering

2012 ◽  
Vol 45 (3) ◽  
pp. 307-312 ◽  
Author(s):  
Takamichi Shinohara ◽  
Tomoko Shirahase ◽  
Daiki Murakami ◽  
Taiki Hoshino ◽  
Moriya Kikuchi ◽  
...  
Keyword(s):  
Thin Film ◽  
Synchrotron Radiation ◽  
Small Angle ◽  
Polymer Thin Film ◽  
X Ray ◽  
X Ray Scattering ◽  
Nondestructive Characterization ◽  
Ray Scattering

Comparative Characterization of Carbon Adsorbents and Polymer Precursors by Small-Angle X-ray Scattering and Nitrogen Adsorption Methods

2011 ◽  
Vol 115 (21) ◽  
pp. 10727-10735 ◽  
Author(s):  
V. M. Gun’ko ◽  
S. T. Meikle ◽  
O. P. Kozynchenko ◽  
S. R. Tennison ◽  
F. Ehrburger-Dolle ◽  
...  
Keyword(s):  
Small Angle ◽  
Nitrogen Adsorption ◽  
Carbon Adsorbents ◽  
X Ray ◽  
Comparative Characterization ◽  
Polymer Precursors ◽  
X Ray Scattering ◽  
Ray Scattering
Sign in / Sign up

Export Citation Format

Share Document