Characterisation of Microstructure as a Systematic Approach to High Strength Cements

1984 ◽  
Vol 42 ◽  
Author(s):  
Karen L. Scrivener ◽  
K. D. Baldie ◽  
Yick Halse ◽  
P. L. Pratt

AbstractUltimately the strength of cement is determined by the properties, amounts and distributions of the phases it contains and by the'way these are bonded together. Here an example is presented of the determination of the amount and distribution of calcium hydroxide, by BEI and quantitative image analysis, in a cement paste and cement/fly ash mixture which had previously been studied by TGA. Examination of crack paths on BEIs of polished cement surfaces gives some indication as to the importance of calcium hydroxide in determining the properties of the cement.

1994 ◽  
Vol 370 ◽  
Author(s):  
Yuting Wang ◽  
Sidney Diamond

AbstractCement paste microstructure as revealed in backscatter SEM presents a number of inherent difficulties that interfere with implementing quantitative image analysis. An approach to overcoming these difficulties is presented, involving gray scale segmentation coupled with application of a hole filling algorithm. Using this approach it is possible to isolate the unhydrated and hydrated portions of phenograins separately, and to combine them for analysis of combined phenograins. Pores and coarse calcium hydroxide masses may also be isolated for feature analysis. Results are reported on mature cement pastes prepared at two water:cement ratios (w:c 0.45 and w:c 0.30) and with and without superplasticizer. It was found that superplasticizer greatly reduced the content and the average size of “visible pores” and increased the content and the average size of coarse CH particles compared to corresponding plain pastes. The area per hydrated phenograin was much smaller in the lower w:c ratio pastes and higher in superplasticized pastes. Among the solid features measured, unhydrated cement particles had the smallest circularity values (at about 2.7) and were the most circular features; Hydrated phenograins had the largest circularity values (at 3.5) and were the most elongated features.


1992 ◽  
Vol 6 (2) ◽  
pp. 153
Author(s):  
G.W. Roberts ◽  
S.M. Gentleman ◽  
B.J. Williams ◽  
C.J. Bruton ◽  
V. Vucicevic ◽  
...  

1993 ◽  
Vol 99 (6) ◽  
pp. 736-740 ◽  
Author(s):  
Patrick A. Jordan ◽  
Billie-Jo M. Kerns ◽  
Jeffrey C. Pence ◽  
Matthew F. Kohler ◽  
Robert C. Bast ◽  
...  

1987 ◽  
Vol 48 (C3) ◽  
pp. C3-521-C3-526 ◽  
Author(s):  
N. THORNE ◽  
A. DUBUS ◽  
J. M. LANG ◽  
F. DEGREVE ◽  
P. MEYER

1994 ◽  
Vol 101 (2) ◽  
pp. 192-197 ◽  
Author(s):  
Billie-Jo M. Kerns ◽  
Patrick A. Jordan ◽  
Lorin L. Faerman ◽  
Andrew Berchuck ◽  
Robert C. Bast ◽  
...  

1987 ◽  
Vol 114 ◽  
Author(s):  
Karen L. Scrivener ◽  
Alison K. Crumbie ◽  
P. L. Pratt

ABSTRACTThe application of quantitative image analysis to the measurenent of microstructural gradients in the interfacial zone in concrete is described. Some preliminary results are presented and discussed.


1995 ◽  
Vol 1 (6) ◽  
pp. 362-371 ◽  
Author(s):  
Lester J. Layfield ◽  
Billie-Jo M. Kerns ◽  
Debbi H. Conlon ◽  
J. Dirk Iglehart ◽  
Jeffrey R Marks ◽  
...  

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