β-D-galactopyranoside Seco-phytoporphyrin from Atropa Belladonna and Solanum Tuberosum Yellow Leaves Determined by Nuclear Magnetic Resonance

Solanum Tuberosum ◽

Nmr Spectroscopy ◽

Magnetic Resonance ◽

Column Chromatography ◽

Atropa Belladonna ◽

Structure Confirmation ◽

Chlorophyll Catabolite ◽

The study described the isolation of β-D-galactopyranoside seco-phytoporphyrin from Atropa belladonna and Solanum tuberosum yellow leaves. Column chromatography was applied for its isolation. The UV-Vis, mass spectrometry and NMR spectroscopy were used for the structure confirmation. The results demonstrate that the two plants that the same chlorophyll catabolite structure.

Combining Mass Spectrometry (MS) and Nuclear Magnetic Resonance (NMR) Spectroscopy for Integrative Structural Biology of Protein–RNA Complexes

Cold Spring Harbor Perspectives in Biology ◽

10.1101/cshperspect.a032359 ◽

2019 ◽

Vol 11 (7) ◽

pp. a032359 ◽

Cited By ~ 3

Author(s):

Alexander Leitner ◽

Georg Dorn ◽

Frédéric H.-T. Allain

Keyword(s):

Mass Spectrometry ◽

Nmr Spectroscopy ◽

Magnetic Resonance ◽

Structural Biology ◽

Integrative Structural Biology ◽

Rna Complexes ◽

Eine ungewöhnliche intramolekulare Photoreaktion eines Hexachlorhexahydromethanonaphthalins / An Unusual Intramolecular Photoreaction of a Hexachlorohexahydromethanonaphthaline

Zeitschrift für Naturforschung B ◽

10.1515/znb-1978-1242 ◽

1978 ◽

Vol 33 (12) ◽

pp. 1563-1564

Author(s):

H. Parlar

Keyword(s):

Mass Spectrometry ◽

Infrared Spectroscopy ◽

Magnetic Resonance ◽

Spectral Data ◽

Column Chromatography ◽

Photoreactions of 2-exo-bromo-5,6,7,8,9,9- hexachloro-1,2,4 a, 5,8,8 a-hexahydro-5,8-methanonaphthaline (1) were studied in the presence of acetophenone. With the help of column chromatography an unusual isomerisation product (3) was isolated, whose structure was established by spectral data obtained by mass spectrometry, infrared spectroscopy, and 1H nuclear magnetic resonance measurements.

Special Issue: NMR-Based Metabolomics

Molecules ◽

10.3390/molecules26113283 ◽

2021 ◽

Vol 26 (11) ◽

pp. 3283

Author(s):

Miriam Pérez-Trujillo ◽

Toby J. Athersuch

Keyword(s):

Mass Spectrometry ◽

Nmr Spectroscopy ◽

Magnetic Resonance ◽

Dynamic Range ◽

Chemical Information ◽

Special Issue ◽

The Core ◽

Analytical Platforms ◽

Nuclear magnetic resonance (NMR) spectroscopy remains one of the core analytical platforms for metabolomics, providing complementary chemical information to others, such as mass spectrometry, and offering particular advantages in some areas of research on account of its inherent robustness, reproducibility, and phenomenal dynamic range [...]

Biomedical applications of directly-coupled chromatography–nuclear magnetic resonance (NMR) spectroscopy and mass spectrometry (MS)

Bioanalytical Separations - Handbook of Analytical Separations ◽

10.1016/s1567-7192(03)80011-6 ◽

2003 ◽

pp. 293-329 ◽

Cited By ~ 2

Author(s):

John C. Lindon ◽

Nigel J.C. Bailey ◽

Jeremy K. Nicholson ◽

Ian D. Wilson

Keyword(s):

Mass Spectrometry ◽

Nmr Spectroscopy ◽

Magnetic Resonance ◽

Biomedical Applications ◽

A Revised Structure for the Glycolipid Terminus of Escherichia coli K5 Heparosan Capsular Polysaccharide

Biomolecules ◽

10.3390/biom10111516 ◽

2020 ◽

Vol 10 (11) ◽

pp. 1516

Author(s):

Lufeng Yan ◽

Li Fu ◽

Ke Xia ◽

Shiguo Chen ◽

Fuming Zhang ◽

...

Keyword(s):

Mass Spectrometry ◽

Escherichia Coli ◽

Nmr Spectroscopy ◽

Magnetic Resonance ◽

Capsular Polysaccharide ◽

Enzymatic Digestion ◽

The structure of heparosan capsular polysaccharide (CPS) has been determined using enzymatic digestion with nuclear magnetic resonance (NMR) spectroscopy and mass spectrometry. Previous errors in the assignment of the glycolipid acceptor structure, from which heparosan is extended, have been corrected. The structure of heparosan CPS is GlcNAc α-1,[4GlcA β-1,4GlcNAc α-1,]n4GlcA β-1,[4Kdo β-2,7Kdo β-2,]0 or 14Kdo β-2,7Kdo β-2,4Kdo β-2,7Kdo β-2,4Kdo β-2,7Kdo β-2,4Kdo β-PG-I (C16:0 or C18:0) (where n is ~250 for a CPS of 100 kDa).

Notizen: Eine nicht erwartete intramolekulare Photoreaktion eines Hexachloroctahydrodimethanonaphthalins/An Unexpected Intramolecular Photoreaction of a Hexachlorooctahydrodimethanonaphthaline

Zeitschrift für Naturforschung B ◽

10.1515/znb-1981-0127 ◽

1981 ◽

Vol 36 (1) ◽

pp. 125-126 ◽

Cited By ~ 1

Author(s):

H. Parlar ◽

Y. Inanici

Keyword(s):

Mass Spectrometry ◽

Infrared Spectroscopy ◽

Magnetic Resonance ◽

Spectral Data ◽

Column Chromatography ◽

Abstract Photoreactions of 1,2,3,4,10,10-hexachloro-6,7-epoxy-1,4,4a,5,6,7,8,8a-octahydro-1,4-endo, endo-5,8-dimethano-naphthaline (1) were studied in acetone with wavelengths above 290 nm. With the help of column chromatography an unusual isomerisation product (4) could be isolated, whose structure was established by spectral data obtained by mass spectrometry infrared spectroscopy, 1H and 13C nuclear magnetic resonance measurements.