scholarly journals RADIATION DAMAGE STUDY OF TYPE 304 STAINLESS STEEL BY HIGH VOLTAGE ELECTRON MICROSCOPY.

1972 ◽  
Author(s):  
G. Das ◽  
T. E. Mitchell
Author(s):  
Gopal Das ◽  
Terence E. Mitchell

In recent years high voltage electron microscopy has found widespread application to simulate the kind of damage produced by neutrons in potential nuclear reactor materials and to study ‘in-situ’ the nucleation and growth of defect clusters, such as dislocation loops and voids.In this investigation AISI Type 304 stainless steel has been used as a prototype to study electron irradiation damage as a function of accelerating voltage, irradiation time and temperature. A preliminary result on such studies will be reported here. 0.4 mm thick discs were cut from as-received 3 mm rods. They were sand-ground to 0.2 mm and most of them were encapsulated in a quartz tube under a vacuum of 10−5 torr and subsequently annealed at 1100°C for 7 hours. Electron transparent foils were made from annealed and as-received discs by a two-step process of jet dimpling and electropolishing.


1972 ◽  
Author(s):  
E. E. Bloom ◽  
J. O. Stiegler ◽  
C. J. McHargue

Author(s):  
A. Ishikawa ◽  
C. Morita ◽  
M. Hibino ◽  
S. Maruse

One of the problems which are met in conventional transmission electron microscopy (CTEM) at high voltages is the reduction of the sensitivity of photographic films for high energy electron beams, resulting in the necessity of using high beam current. This cancels out an advantage of high voltage electron microscopy which is otherwise expected from the reduction of the inelastic scattering in the specimen, that is the reduced radiation damage of the specimen during observations. However, it is expected that the efficiency of the detector of scanning transmission electron microscopy (STEM) can be superior to that of CTEM, since the divergence of the electron beam in the detecting material does not affect the quality of the image. In addition to observation with less radiation damage, high voltage STEM with high detection efficiency is very attractive for observations of weak contrast objects since the enhancement of the contrast (which is an important advantage of STEM) is easily realized electrically.


1972 ◽  
Vol 14 (3-4) ◽  
pp. 231-243 ◽  
Author(s):  
E. E. Bloom ◽  
J. O. Stiegler ◽  
C. J. McHargue

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