A Facile Microwave-Assisted Solution Combustion Synthesis of Highly Stable Magnesium Oxide for Multicomponent Mannich Reaction

2012 ◽  
Vol 1 (3) ◽  
pp. 164-170 ◽  
Author(s):  
Lankela H. Reddy ◽  
Gunugunuri K. Reddy ◽  
Boningari Thirupathi ◽  
Benjaram M. Reddy
Keyword(s):  
Combustion Synthesis ◽  
Magnesium Oxide ◽  
Mannich Reaction ◽  
Solution Combustion Synthesis ◽  
Solution Combustion ◽  
Microwave Assisted

Microwave-Assisted Solution Combustion Synthesis and Characterization of Thermoelectric Ca3Co2O6 Powders

2013 ◽  
Vol 802 ◽  
pp. 84-88
Author(s):  
Sagulthai Kahatta ◽  
Nopsiri Chaiyo ◽  
Chesta Ruttanapun ◽  
Wicharn Techitdheera ◽  
Wisanu Pecharapa ◽  
...  
Keyword(s):  
Combustion Synthesis ◽  
Solution Combustion Synthesis ◽  
Molar Ratio ◽  
X Ray Diffraction ◽  
Solution Combustion ◽  
X Ray ◽  
Microwave Assisted ◽  
Product Characterization ◽  
Rhombohedral Crystal Structure ◽  
Rhombohedral Crystal

The microwave-assisted solution combustion synthesis was applied to the initial synthesizing of Ca3Co2O6powder using glycine as a fuel and nitrate as an oxidant. The as-synthesized powders were calcined at 700-1,000ºC for 4h. Product characterization was performed using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and Scanning electron microscope (SEM). The fuel-to-oxidizer molar ratio was found to affect the combustion reaction and character of the powder obtained. The phase composition of powder after calcination at various temperatures has shown that the formation of Ca3Co2O6occurs directly. The calcined powder possesses a rhombohedral crystal structure with an X-ray diffraction pattern that could be matched with the Ca3Co2O6JCPDS: 89-0629. This method is a simple way of synthesizing fine Ca3Co2O6powder with a low calcination temperature.

Mechanistic insights into defect chemistry and tailored photo-luminescent and photo-catalytic properties of aliovalent cations substituted Zn0.94M0.06-x LixO (M: Fe3+, Al3+, Cr3+) nanoparticles

2021 ◽  
Author(s):  
Sajid A Ansari ◽  
C. Manjunatha ◽  
Nazish Parveen ◽  
SHIVRAJ BW ◽  
Hari Krishna Rajan
Keyword(s):  
Combustion Synthesis ◽  
Catalytic Properties ◽  
Solution Combustion Synthesis ◽  
Structural Features ◽  
Defect Chemistry ◽  
Photocatalytic Properties ◽  
Solution Combustion ◽  
Microwave Assisted ◽  
Photo Luminescent

In this work, we demonstrate the microwave assisted solution combustion synthesis of aliovalent cations substituted Zn0.94M0.06-xLixO (M: Fe3+, Al3+, Cr3+) nanoparticles. The structural features, photoluminscent and photocatalytic properties were characterized...

Formation of nanostructured fluorapatite via microwave assisted solution combustion synthesis

2014 ◽  
Vol 37 ◽  
pp. 363-368 ◽  
Author(s):  
Maryam Nabiyouni ◽  
Huan Zhou ◽  
Timothy J.F. Luchini ◽  
Sarit B. Bhaduri
Keyword(s):  
Combustion Synthesis ◽  
Solution Combustion Synthesis ◽  
Solution Combustion ◽  
Microwave Assisted
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