scholarly journals Mutual Verification of Phase Fraction Analysis Techniques for Steels Comprising Deformation Induced Martensite Phases: Neutron-Diffraction-Based Rietveld Texture Analysis and Saturation Magnetization Measurement

2020 ◽  
Vol 106 (7) ◽  
pp. 457-464 ◽  
Author(s):  
Yusuke Onuki ◽  
Takuro Masumura ◽  
Toshihiro Tsuchiyama ◽  
Shigeo Sato ◽  
Toshiro Tomida ◽  
...  
2017 ◽  
Vol 52 (19) ◽  
pp. 11643-11658 ◽  
Author(s):  
Yusuke Onuki ◽  
Akinori Hoshikawa ◽  
Shigeo Sato ◽  
Toru Ishigaki ◽  
Toshiro Tomida

2010 ◽  
Vol 25 (3) ◽  
pp. 283-296 ◽  
Author(s):  
H.-R. Wenk ◽  
L. Lutterotti ◽  
S. C. Vogel

One of the advantages of a multidetector neutron time-of-flight diffractometer such as the high pressure preferred orientation diffractometer (HIPPO) at the Los Alamos Neutron Science Center is the capability to measure efficiently preferred orientation of bulk materials. A routine experimental method for measurements, both at ambient conditions, as well as high or low temperatures, has been established. However, only recently has the complex data analysis been streamlined to make it straightforward for a noninitiated user. Here, we describe the Rietveld texture analysis of HIPPO data with the computer code Materials Analysis Using Diffraction (MAUD) as a step-by-step procedure and illustrate it with a metamorphic quartz rock. Postprocessing of the results is described and neutron diffraction results are compared with electron backscatter diffraction measurements on the same sample.


Author(s):  
Kenichi Maruyama ◽  
Seiya Tanaka ◽  
Ryoji Kiyanagi ◽  
Akiko Nakao ◽  
Kentaro Moriyama ◽  
...  

1993 ◽  
Vol 21 (2-3) ◽  
pp. 71-78
Author(s):  
H.-G. Brokmeier

This paper describes the application of neutron diffraction to investigate the texture of a zinc layer 8 μm in thickness. In a nondestructive way both the texture of the zinc layer as well as the texture of the steel substrate were studied. Therefore, pole figures of iron ((110), (200) and (211)) and of zinc ((0002), (101¯0), (101¯1); and (101¯3)/(112¯0)) were measured; additionally the orientation distribution function of iron and zinc were calculated.


2005 ◽  
Vol 17 (1) ◽  
pp. 102-106 ◽  
Author(s):  
Emmanuel Guilmeau ◽  
Daniel Chateigner ◽  
Tohru S. Suzuki ◽  
Yoshio Sakka ◽  
Catherine Henrist ◽  
...  

2007 ◽  
Vol 90 (1) ◽  
pp. 9-14 ◽  
Author(s):  
R. Arletti ◽  
L. Cartechini ◽  
R. Rinaldi ◽  
S. Giovannini ◽  
W. Kockelmann ◽  
...  

2004 ◽  
Vol 443-444 ◽  
pp. 267-270 ◽  
Author(s):  
H. Sitepu ◽  
Heinz Günter Brokmeier

The orientation distribution function (ODF) of the textured polycrystalline nickel titanium (NiTi) shape memory alloys (SMAs) was determined from the measured austenitic (B2)pole-figures by neutron diffraction. The texture results showed that neutron diffraction is an excellent tool to investigate the minor variation in the texture of NiTi alloys, which is very sensitive to the variation of the content of nickel in the materials. Moreover, the alloys crystallographic phase fraction and texture were calculated from Rietveld refinement with generalized spherical harmonic (GSH) description for the measured complete neutron powder diffraction (ND) spectrum, rather than a few isolated peaks, during in-situ temperature-induced martensitic transformation. The phase fraction results are consistent with the differential scanning calorimeter (DSC) curves.


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