Three-Dimensional Investigations of Finely Grained Materials/ Trójwymiarowa Analiza Materiałów Drobnokrystalicznych
Abstract Development of new materials requires application of sophisticated techniques to characterize microstructure in a very detailed way. The combination of Electron Backscatter Diffraction (EBSD) and Energy Dispersive Spectrometry (EDS) with Focused Ion Beam (FIB) are excellent examples of such techniques. They are based on serial sectioning of chosen region in the investigated sample followed by data acquisition using the dual-beam scanning electron microscope equipped with both electron and ion columns. Three kinds of samples have been investigated: a) are anticorrosive Ni-Mo coating on ferritic steel; b) the oxidized Crofer22 APU ferritic stainless steel; c) the Al 6013 aluminum alloy after complex plastic deformation. The obtained results allowed to analyze crystalline morphology, distribution of precipitates as well as to reconstruct internal structure of grains and grains boundaries geometry.