scholarly journals Preparative Separation and Purification of Geniposide from Gardenia jasminoides Ellis fruit Using Macroporous Adsorption Resin D101

2018 ◽  
Vol 42 (1) ◽  
pp. 29-36 ◽  
Author(s):  
Tran Trong Bien ◽  
Bui Thi Thuy Luyen ◽  
Nguyen Van Han
Keyword(s):  
Preparative Separation ◽  
Separation And Purification ◽  
Gardenia Jasminoides ◽  
Macroporous Adsorption Resin ◽  
Adsorption Resin ◽  
Gardenia Jasminoides Ellis

scholarly journals The Separation and Purification of Ellagic Acid from Phyllanthus urinaria L. by a Combined Mechanochemical-Macroporous Resin Adsorption Method

Separations ◽  
2021 ◽  
Vol 8 (10) ◽  
pp. 186
Author(s):  
Zili Guo ◽  
Shuting Xiong ◽  
Yuanyuan Xie ◽  
Xianrui Liang
Keyword(s):  
Ellagic Acid ◽  
Ball Mill ◽  
Separation And Purification ◽  
Macroporous Resin ◽  
Adsorption Method ◽  
Phyllanthus Urinaria ◽  
Wide Range ◽  
Macroporous Adsorption Resin ◽  
Adsorption Resin

Ellagic acid is a phenolic compound that exhibits both antimutagenic and anticarcinogenic activity in a wide range of assays in vitro and in vivo. It occurs naturally in some foods such as raspberries, strawberries, grapes, and black currants. In this study, a valid and reliable method based on mechanochemical-assisted extraction (MCAE) and macroporous adsorption resin was developed to extract and prepare ellagic acid from Phyllanthus urinaria L. (PUL). The MCAE parameters, acidolysis, and macroporous adsorption resin conditions were investigated. The key MCAE parameters were optimized as follows: the milling time was 5 min, the ball mill speed was 100 rpm, and the ball mill filling rate was 20.9%. Sulfuric acid with a concentration of 0.552 mol/L was applied for the acidolysis with the optimized acidolysis time of 30 min and acidolysis temperature of 40 °C. Additionally, the XDA-8D macroporous resin was chosen for the purification work. Both the static and dynamic adsorption tests were carried out. Under the optimized conditions, the yield of ellagic acid was 10.2 mg/g, and the content was over 97%. This research provided a rapid and efficient method for the preparation of ellagic acid from the cheaply and easily obtained PUL. Meanwhile, it is relatively low-cost work that can provide a technical basis for the comprehensive utilization of PUL.

Purification of Total Flavonoids from Buddleja officinalis by AB-8 Macroporous Adsorption Resin

2013 ◽  
Vol 641-642 ◽  
pp. 988-992 ◽  
Author(s):  
Ying Wen ◽  
Ya Ting Liu ◽  
Jing Min Zhang ◽  
Lei Guo
Keyword(s):  
Flow Rate ◽  
Ph Value ◽  
Total Flavonoids ◽  
Separation And Purification ◽  
Sample Flow Rate ◽  
Macroporous Adsorption Resin ◽  
Adsorption Resin

The separation and purification of total flavonoids from Buddleja officinalis were carried out by AB-8 macroporous adsorption resin. The optimum adsorption conditions for sample flow rate, pH value and feeding concentration were 2.0 mL/min, 4.5 and 1.6 mg/mL, respectively, and the optimum desorption conditions were obtained by using 2.0 BV of 70% ethanol as desorption solvent at a flow rate of 1.0 mL/min. Under these conditions, the flavonoids content of the final product was 90.43%, increased by 1.7 times than unpurified sample (53.09%).

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