scholarly journals Isolation and Characterization of Nanocrystalline Cellulose Isolated from Pineapple Crown Leaf Fiber Agricultural Wastes Using Acid Hydrolysis

Polymers ◽  
2021 ◽  
Vol 13 (23) ◽  
pp. 4188
Author(s):  
Fitriani Fitriani ◽  
Sri Aprilia ◽  
Nasrul Arahman ◽  
Muhammad Roil Bilad ◽  
Amri Amin ◽  
...  

Pineapple crown leaf fiber (PCLF) is one of the major biomass wastes from pineapple processing plants. It consists mostly of carbohydrate polymers, such as cellulose, hemicellulose, and lignin. It can be further processed to form a more valuable and widely used nanocrystalline cellulose (NCC). This study investigates the effect of hydrolysis time on the properties of the produced NCC. The acid hydrolysis was conducted using 1 M of sulfuric acid at hydrolysis times of 1–3 h. The resulting NCCs were then characterized by their morphology, functional groups, crystallinity, thermal stability, elemental composition, and production yield. The results show that the NCC products had a rod-like particle structure and possessed a strong cellulose crystalline structure typically found in agricultural fiber-based cellulose. The highest NCC yield was obtained at 79.37% for one hour of hydrolysis. This NCC also displayed a higher decomposition temperature of 176.98 °C. The overall findings suggest that PCLF-derived NCC has attractive properties for a variety of applications.

2017 ◽  
Vol 2 (2) ◽  
pp. 103-108 ◽  
Author(s):  
N. A. Sri Aprilia ◽  
Aulia Chintia Ambarita ◽  
Karmila Karmila ◽  
M. Adam Armando ◽  
Faisal Yusupi Guswara

Sugarcane bagass was used as effect of hydrolysis time for isolation of cellulose nanofiber (CNF) was done. The other components such as lignin and hemicellulose were removed from the biomass by adding NaOH and NaOCl and continue to synthesist of CNF has done using formic acid hydrolysis wiht addition of ferric chloride catalyst. FTIR analysis showed that were no significant variations in peak positions, This result did not affect the chemical compounds of CNF. XRD analysis showed increase the hydrolisis time also increase the crystallinity percentage and crystalline size. Increasing hydrolysis time would decreased the percentage yield of CNF.


2020 ◽  
Vol 24 (4) ◽  
pp. 374-379
Author(s):  
Syed Farooq Adil ◽  
Vanita S. Bhat ◽  
Khalid Mujasam Batoo ◽  
Ahamad Imran ◽  
Mohamed E. Assal ◽  
...  

2013 ◽  
Vol 59 (1) ◽  
pp. 39-45 ◽  
Author(s):  
Chao Gong ◽  
Spencer Heringa ◽  
Randhir Singh ◽  
Jinkyung Kim ◽  
Xiuping Jiang

The objectives of this study were to isolate and characterize bacteriophages specific to hydrogen-sulfide-producing bacteria (SPB) from raw animal materials, and to develop a SPB-specific bacteriophage cocktail for rendering application. Meat, chicken offal, and feather samples collected from local supermarkets and rendering processing plants were used to isolate SPB (n = 142). Bacteriophages (n = 52) specific to SPB were isolated and purified from the above samples using 18 of those isolated SPB strains as hosts. The host ranges of bacteriophages against 5 selected SPB strains (Escherichia coli, Citrobacter freundii, and Hafnia alvei) were determined. Electron microscopy observation of 9 phages selected for the phage cocktail revealed that 6 phages belonged to the family of Siphoviridae and 3 belonged to the Myoviridae family. Restriction enzyme digestion analysis with endonuclease DraI detected 6 distinguished patterns among the 9 phages. Phage treatment prevented the growth of SPB for up to 10 h with multiplicity of infection ratios of 1, 10, 100, and 1000 in tryptic soy broth at 30 °C, and extended the lag phase of SPB growth for 2 h at 22 °C with multiplicities of infection of 10, 100, and 1000. These results suggest that the selected bacteriophage cocktail has a high potential for phage application to control SPB in raw animal materials destined for the rendering process.


2012 ◽  
Vol 33 (5) ◽  
pp. 764-772 ◽  
Author(s):  
G.M. Arifuzzaman Khan ◽  
S.R. Shahrear Palash ◽  
M. Shamsul Alam ◽  
A.K. Chakraborty ◽  
M.A. Gafur ◽  
...  

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