Qualitative identification of impurities and principal component quantitative analysis of zearalanone on purity certified reference material

2019 ◽  
Vol 37 (8) ◽  
pp. 911
Author(s):  
Mengyu FENG ◽  
Shuan LIU ◽  
Yan GAO ◽  
Shukun ZHOU ◽  
Zhen GUO ◽  
...  
Author(s):  
J. M. Paque ◽  
R. Browning ◽  
P. L. King ◽  
P. Pianetta

Geological samples typically contain many minerals (phases) with multiple element compositions. A complete analytical description should give the number of phases present, the volume occupied by each phase in the bulk sample, the average and range of composition of each phase, and the bulk composition of the sample. A practical approach to providing such a complete description is from quantitative analysis of multi-elemental x-ray images.With the advances in recent years in the speed and storage capabilities of laboratory computers, large quantities of data can be efficiently manipulated. Commercial software and hardware presently available allow simultaneous collection of multiple x-ray images from a sample (up to 16 for the Kevex Delta system). Thus, high resolution x-ray images of the majority of the detectable elements in a sample can be collected. The use of statistical techniques, including principal component analysis (PCA), can provide insight into mineral phase composition and the distribution of minerals within a sample.


2011 ◽  
Vol 400 (3) ◽  
pp. 821-833 ◽  
Author(s):  
Pearse McCarron ◽  
Håkan Emteborg ◽  
Cíara Nulty ◽  
Thomas Rundberget ◽  
Jared I. Loader ◽  
...  

Molecules ◽  
2021 ◽  
Vol 26 (14) ◽  
pp. 4370
Author(s):  
Liping Fang ◽  
Linyan Huang ◽  
Gang Yang ◽  
Yang Jiang ◽  
Haiping Liu ◽  
...  

Water matrix certified reference material (MCRM) of volatile organic compounds (VOCs) is used to provide quality assurance and quality control (QA/QC) during the analysis of VOCs in water. In this research, a water MCRM of 28 VOCs was developed using a “reconstitution” approach by adding VOCs spiking, methanol solution into pure water immediately prior to analysis. The VOCs spiking solution was prepared gravimetrically by dividing 28 VOCs into seven groups, then based on ISO Guide 35, using gas chromatography-mass spectrometry (GC-MS) to investigate the homogeneity and long-term stability. The studies of homogeneity and long-term stability indicated that the batch of VOCs spiking solution was homogeneous and stable at room temperature for at least 15 months. Moreover, the water MCRM of 28 VOCs was certified by a network of nine competent laboratories, and the certified values and expanded uncertainties of 28 VOCs ranged from 6.2 to 17 μg/L and 0.5 to 5.3 μg/L, respectively.


MAPAN ◽  
2017 ◽  
Vol 32 (3) ◽  
pp. 215-222
Author(s):  
H. E. Ahmed ◽  
Mohamed Hassan ◽  
Mohamed Nour ◽  
A. B. Shehata ◽  
Maher Helmy

2010 ◽  
Vol 53 (4) ◽  
pp. 1037-1041 ◽  
Author(s):  
Sooyeun Lee ◽  
Hajime Miyaguchi ◽  
Eunyoung Han ◽  
Eunmi Kim ◽  
Yonghoon Park ◽  
...  

2010 ◽  
Vol 286 (1) ◽  
pp. 121-127 ◽  
Author(s):  
M. K. Pham ◽  
M. Betti ◽  
P. P. Povinec ◽  
V. Alfimov ◽  
D. Biddulph ◽  
...  

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