Structural Characterization of Erbium doped LAS Glass Ceramic Obtained by Glass Melting Technique

Author(s):  
R. Krsmanović ◽  
Giovanni Bertoni ◽  
G. Van Tendeloo
2007 ◽  
Vol 555 ◽  
pp. 377-381
Author(s):  
R. Krsmanović ◽  
Giovanni Bertoni ◽  
Gustaaf Van Tendeloo

Samples of transparent glass-ceramics in the ternary system Li2O-Al2O3-SiO2 (LAS), with Er2O3 as a luminescent dopant, are investigated. The initial glass is obtained by the classical melting technique. In order to induce ceramization of the glass, TiO2 and ZrO2 are added in small amount as nucleating agents. The thermal treatments at 730 and 770°C are carried out to promote formation of titanium zirconate solid solution precipitates. The spatial distribution of the precipitates in the material, their morphology, and their composition are investigated with TEM, HRTEM, HAADF-STEM, EELS and EFTEM. The results demonstrate that with the glass-melting preparation technique it is possible to achieve small nanoparticles with uniform distribution and higher number density than with the sol-gel glass preparation.


2012 ◽  
Author(s):  
Valérie Mauroy ◽  
Wilfried Blanc ◽  
Michèle Ude ◽  
Stanislaw Trzesien ◽  
Bernard Dussardier ◽  
...  

2008 ◽  
Vol 55 ◽  
pp. 68-73 ◽  
Author(s):  
Simone Berneschi ◽  
M. Brenci ◽  
Gualtiero Nunzi Conti ◽  
Stefano Pelli ◽  
G.C. Righini ◽  
...  

Erbium-doped tellurite glasses show great potential for the fabrication of high-performance integrated optical amplifiers and lasers, thanks to their unique properties in terms of bandwidth and rare earth solubility. As a first step towards the development of smart multi-functional integrated optical circuits, the fabrication of multimode channel waveguides in a sodium-tungsten-tellurite glass, by using nitrogen ions implantation, has been recently demonstrated [1]. The effects of the ion implantation process, however, have not been fully clarified, and a deeper investigation would be necessary in order to optimize the process and to truly exploit the glass useful characteristics. We therefore report here the results of a broad optical, topographic, and structural characterization of tellurite samples irradiated with various doses of nitrogen ions, while keeping constant the beam energy at 1.5 MeV. Characterization techniques have included absorption and luminescence spectroscopy, modal (dark-line) spectroscopy, surface profilometry, scanning electron microscopy, cathodoluminescence spectroscopy and EDX analysis.


2013 ◽  
Vol 3 (6) ◽  
pp. 884 ◽  
Author(s):  
Indumathi Kamma ◽  
Monday Mbila ◽  
Karen E. Steege Gall ◽  
B. Rami Reddy

1992 ◽  
Vol 121 (1-2) ◽  
pp. 121-131 ◽  
Author(s):  
I. Poole ◽  
K.E. Singer ◽  
A.R. Peaker ◽  
A.C. Wright

2014 ◽  
Vol 37 ◽  
pp. 87-92
Author(s):  
Kevin Bourhis ◽  
Yaroslav Shpotyuk ◽  
Jonathan Massera ◽  
Ville Aallos ◽  
Thierry Jouan ◽  
...  

2006 ◽  
Vol 27 (10) ◽  
pp. 1092-1096 ◽  
Author(s):  
Senol Yılmaz ◽  
Gunhan Bayrak ◽  
Saduman Sen ◽  
Ugur Sen

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