The Synthesis and Photocatalytic Properties of ZnO-SnO2 Nanorods Using Bamboo Charcoal as the Template

2014 ◽  
Vol 1014 ◽  
pp. 21-24
Author(s):  
Wei Liu ◽  
Jian Fa Ou ◽  
Qiu Ying Pan ◽  
Wu Yi Zhou

The ZnO-SnO2 nanorods were prepared successfully by wet chemical method and bamboo charcoal as the template. The transmission electron microscope (TEM) results showed that the ZnO-SnO2 nanorods prepared at 700°C were uniform with the diameters of about 55 nm and the lengths of about 160 nm. The photocatalytic activity was studied while the methylene blue was used as the organic pollutant. The results indicate that the degradation rate of the methylene blue by the ZnO-SnO2 nanorods was about 89%, twice higher than that of the pure ZnO nanomaterials.

2017 ◽  
Vol 8 ◽  
pp. 1257-1265 ◽  
Author(s):  
Urszula Klekotka ◽  
Magdalena Rogowska ◽  
Dariusz Satuła ◽  
Beata Kalska-Szostko

Ferrite nanoparticles with nominal composition Me0.5Fe2.5O4 (Me = Co, Fe, Ni or Mn) have been successfully prepared by the wet chemical method. The obtained particles have a mean diameter of 11–16 ± 2 nm and were modified to improve their magnetic properties and chemical activity. The surface of the pristine nanoparticles was functionalized afterwards with –COOH and –NH2 groups to obtain a bioactive layer. To achieve our goal, two different modification approaches were realized. In the first one, glutaraldehyde was attached to the nanoparticles as a linker. In the second one, direct bonding of such nanoparticles with a bioparticle was studied. In subsequent steps, the nanoparticles were immobilized with enzymes such as albumin, glucose oxidase, lipase and trypsin as a test bioparticles. The characterization of the nanoparticles was acheived by transmission electron microscopy, X-ray diffraction, energy dispersive X-ray and Mössbauer spectroscopy. The effect of the obtained biocomposites was monitored by Fourier transform infrared spectroscopy. The obtained results show that in some cases the use of glutaraldehyde was crucial (albumin).


2014 ◽  
Vol 5 ◽  
pp. 639-650 ◽  
Author(s):  
Sini Kuriakose ◽  
Vandana Choudhary ◽  
Biswarup Satpati ◽  
Satyabrata Mohapatra

We report the synthesis of Ag–ZnO hybrid plasmonic nanostructures with enhanced photocatalytic activity by a facile wet-chemical method. The structural, optical, plasmonic and photocatalytic properties of the Ag–ZnO hybrid nanostructures were studied by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), photoluminescence (PL) and UV–visible absorption spectroscopy. The effects of citrate concentration and Ag nanoparticle loading on the photocatalytic activity of Ag–ZnO hybrid nanostructures towards sun-light driven degradation of methylene blue (MB) have been investigated. Increase in citrate concentration has been found to result in the formation of nanodisk-like structures, due to citrate-assisted oriented attachment of ZnO nanoparticles. The decoration of ZnO nanostructures with Ag nanoparticles resulted in a significant enhancement of the photocatalytic degradation efficiency, which has been found to increase with the extent of Ag nanoparticle loading.


2013 ◽  
Vol 1506 ◽  
Author(s):  
L. Wang ◽  
B. K. Rai ◽  
S. R. Mishra

AbstractNanostructured Al3+ doped Ni0.75Zn0.25Fe2-xAlxO4 (x = 0.0,0.2,0.4,0.6,0.8, and 1.0) ferrites were synthesized via wet chemical method. X-ray diffraction, transmission electron microscopy, and magnetization measurements have been used to investigate the structural and magnetic properties of spinel ferrites calcined at 950 °C .With the doping of Al3+, the particle size of Ni0.75Zn0.25Fe2-xAlxO4 first increased to 47 nm at x = 0.4 and then decreased down to 37 nm at x = 1. Saturation magnetization decreased linearly with Al3+ due to magnetic dilution. The coercive field showed an inverse dependence on the particle size of ferrites.


Author(s):  
Nguyen Ca ◽  
N. D Vinh ◽  
Phan Van Do ◽  
N. T. Hien ◽  
Xuan Hoa Vu ◽  
...  

Tb3+-doped ZnSe quantum dots (QDs) with Tb content in the range of 0.5 - 7% were successfully synthesized by a wet chemical method. X-ray diffraction (XRD) and transmission electron microscopy...


Author(s):  
Jianping Ai ◽  
Weixiu Liao ◽  
Zehua Zhou ◽  
Lihong Cheng ◽  
Zhiqin Chen ◽  
...  

2011 ◽  
Vol 328-330 ◽  
pp. 1139-1142 ◽  
Author(s):  
Pei Yan Ma ◽  
Yan Wu ◽  
Zheng Yi Fu ◽  
Wei Min Wang

A new type of ZnO/Ag micro hybrid material has been fabricated by a facile wet chemical method using citrate as a crystal growth modifier. The morphology and component of ZnO/Ag hybrid material were characterized by SEM and XRD. It is shown that the platelike crystals connect together by means of embedding. The sample is composed of wurtzite ZnO and face-centered cubic Ag. The results of XPS, UV-Vis and PL spectra verify the electron transfer from Ag to ZnO. The photocatalytic test with Rhodamine B (RhB) as a representative dye pollutant shows that the ZnO/Ag hybrid material exhibits an improved photocatalytic activity.


2007 ◽  
Vol 92 (2) ◽  
pp. 239-246 ◽  
Author(s):  
Hong Li ◽  
Baolin Zhu ◽  
Yunfeng Feng ◽  
Shurong Wang ◽  
Shoumin Zhang ◽  
...  

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