Comparison of Spark Plasma Sintering and Hot Pressing of MgAlON

2007 ◽  
Vol 336-338 ◽  
pp. 1060-1061 ◽  
Author(s):  
Qing Huang ◽  
Hou Xing Zhang ◽  
Yong Huang ◽  
Hai Feng Li ◽  
Zhi Jian Wan

MgAlON ceramics were prepared by spark plasma sintering (SPS) and hot pressing (HP), respectively. It was found that SPSed MgAlON samples had a single MgAlON phase with almost no open pore while HPed MgAlON had a minor AlN phase. The strength of SPSed samples is higher than 500MP, being much higher than that of the HPed samples. The experimental results revealed that that SPS was a rapid and reliable process for the further development of MgAlON.

2007 ◽  
Vol 534-536 ◽  
pp. 1229-1232
Author(s):  
Li Hui Zhu ◽  
Guang Jie Shao ◽  
Yi Xiong Liu ◽  
Dave Siddle

WC-10Co-0.8VC nanocrystalline powders were sintered by spark plasma sintering (SPS) and hot pressing sintering (HPS), and the microstructure and properties were compared. Results show that, sintered at 1300°C, the sample prepared by SPS for only 3 minutes has higher density than that prepared by HPS for 60 minutes. SEM and SPM observation shows SPS at 1200°C has a more uniform and finer microstructure, and most of the WC grains are smaller than 100nm. It has a relative density of 95.1%, HV30 of 1887, and KIC of 11.5 MPam1/2. If a suitable sintering parameter is chosen, SPS is a promising consolidation technique to prepare nanocrystalline WC-10Co-0.8VC with improved properties.


2011 ◽  
Vol 686 ◽  
pp. 740-744 ◽  
Author(s):  
Yi Long Ma ◽  
Deng Ming Chen ◽  
Qian Shen ◽  
Peng Jun Cao

Bulk isotropic and anisotropic Nd13.5Fe80.4Ga0.5B5.6 and Nd13.5Fe80.4Ga0.5B5.6/Fe magnets were synthesized by applying spark plasma sintering (SPS) technique. The effect of hot-pressing temperature on the magnetic properties of hot-pressed (HP) and hot-deformed (HD) magnets without additive and with 5% Fe addition was investigated. With increasing sintering temperature for HP magnets, the grain grew gradually. For HD magnets, the optimal magnetic properties could be obtained at hot-pressing temperature 680°C due to the development of desired c-axis texture and uniform microstructure, which resulted from the appropriate and uniform grain size in HP magnets. Fe addition could enhance remanence (Br) and magnetic energy products ((BH)m) of HP and HD magnets. However, the maximum magnetic energy product of HD magnets decreased when hot-pressing temperature was higher than 650°C.


2015 ◽  
Vol 51 (10) ◽  
pp. 1047-1053 ◽  
Author(s):  
V. N. Chuvil’deev ◽  
M. S. Boldin ◽  
Ya. G. Dyatlova ◽  
V. I. Rumyantsev ◽  
S. S. Ordanyan

2015 ◽  
Vol 16 (7) ◽  
pp. 712 ◽  
Author(s):  
Andrey V. Smirnov ◽  
Denis I. Yushin ◽  
Igor A. Zverev ◽  
Andrey R. Maslov ◽  
Ramon Torrecillas

2014 ◽  
Vol 11 (2) ◽  
pp. 123-130 ◽  
Author(s):  
D. Sebayang ◽  
Deni Khaerudini ◽  
M. Othman ◽  
S. Hasan ◽  
S. Mahzan ◽  
...  

The oxidation kinetics and microstructure characteristics of oxide scales thermally grown on the surface of developed FeCr alloy were investigated at 900 °C. The influence of difference sintering technique, i.e. spark plasma sintering and hot pressing, to improve nanostructured alloy performance was studied. The La-implantation was also considered in this study. It was found that the SPS sintered sample showed better performance than the HP sintered sample. Moreover, it also found that a combining of La-implantation and nanostructured alloy was most beneficial. While nanostructured alloy reduced the oxidation rate, the La-implantation increased the Cr2O3 scale conductivity.


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