LC-MS Analysis of Low Molecular Weight Carbonyl Compounds as 2,4-Dinitrophenylhydrazones Using Negative Ion Mode Electronspray Ionization Mass Spectrometry

Author(s):  
Akio Yasuhara ◽  
Yuuka Tanaka ◽  
Miyuki Makishima ◽  
Shigeru Suzuki ◽  
Takayuki Shibamoto
Materials ◽  
2021 ◽  
Vol 14 (22) ◽  
pp. 6848
Author(s):  
Małgorzata Kasperkowiak ◽  
Monika Kurowska ◽  
Maciej Zalas ◽  
Rafał Frański

For many applications, TiO2 must have a unique surface structure responsible for its desirable physicochemical properties. Therefore the fast and easy methods of TiO2 surface characterization are of great interest. Heated TiO2 samples and dye-modified TiO2 samples were analyzed by laser desorption/ionization mass spectrometry. In the negative ion mode, two types of ions were detected, namely (TiO2)n− and (TiO2)nOH−. It has been established that the samples can be differentiated based on the relative ion abundances, especially with respect to the free hydroxyl group population. It indicates that laser desorption ionization mass spectrometry has the potential for the investigation of the surface properties of various TiO2 materials.


The Analyst ◽  
2020 ◽  
Vol 145 (7) ◽  
pp. 2811-2811
Author(s):  
Theoneste Muyizere ◽  
Yajun Zheng ◽  
Hongni Liu ◽  
Jia Zhao ◽  
Jin Li ◽  
...  

Correction for ‘Metal salt assisted electrospray ionization mass spectrometry for the soft ionization of GAP polymers in negative ion mode’ by Theoneste Muyizere et al., Analyst, 2020, 145, 34–45.


2014 ◽  
Vol 29 (3) ◽  
pp. 520-528 ◽  
Author(s):  
Yusuke Fukami ◽  
Tetsuya Yokoyama

We present a new method for precise isotope analysis of Te by thermal ionization mass spectrometry in negative ion mode (N-TIMS) along with an improved technique for chemical separation of Te from geochemical samples.


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