scholarly journals Effect of silver doping on structural and photocatalytic circumstances of ZnO nanoparticles

2020 ◽  
pp. 13-20
Author(s):  
Luma Ahmed ◽  
Eitemad S. Fadhil ◽  
Ayad F. Mohammed
Keyword(s):  
Zno Nanoparticles ◽  
Precipitation Method ◽  
Methyl Green ◽  
Zno Nanoparticle ◽  
Zno Nps ◽  
Force Microscopy ◽  
Ft Ir ◽  
Doped Zno ◽  
Co Precipitation ◽  
Artificial Uv

This article describes the synthesis of ZnO nanoparticles (Nps) using the co-precipitation method and then calcinated at 500oC for 2 h. The photo activity of ZnO nanoparticles was examined in photo decolorization of methyl green dye under artificial UV -A light. This prepared photocatalyst (ZnO Np) was modified his surface by 2% Ag doped using the photo deposition method under inert gas for 3h. The characterization of undoped and 2% Ag doped ZnO Nps were estimated by Fourier-transform infrared spectroscopy (FT-IR), X-ray Diffraction (XRD), and Atomic force microscopy (AFM). In FT-IR analysis, the new peaks occurred around 624-778 cm-1 confirmed the Ag really is doped on prepared ZnO Np. Based on data from XRD, the mean crystal size was reduced with doped the 2% Ag. The AFM images for the prepared photocatalysts ensure that the shapes of all samples are semi-spherical with nanometer size. Series of kinetics experiments were performed for the photocatalytic decolourization of methyl green dye using undoped and 2% Ag doped ZnO nanoparticle and found to be pseudo-first-order kinetics.

scholarly journals Electrical behavior and enhanced photocatalytic activity of (Ag, Ni) co-doped ZnO nanoparticles synthesized from co-precipitation technique

2020 ◽  
Vol 81 (6) ◽  
pp. 1296-1307
Author(s):  
R. Jeyachitra ◽  
S. Kalpana ◽  
T. S. Senthil ◽  
Misook Kang
Keyword(s):  
Electron Microscopy ◽  
Photocatalytic Activity ◽  
Zno Nanoparticles ◽  
Uv Light ◽  
Light Exposure ◽  
Precipitation Method ◽  
Zno Nps ◽  
Transmission Electron ◽  
Doped Zno ◽  
Co Precipitation

Abstract Methylene blue (MB) dye is the most common harmful, toxic, and non-biodegradable effluent produced by the textile industries. The present study investigates the effect of zinc oxide (ZnO) nanoparticles (NPs) and Ag–Ni doped ZnO NPs on the performance of photocatalytic degradation of MB dye. Pure ZnO and Ag–Ni doped ZnO NPs are synthesized using the co-precipitation method. The crystalline nature and surface morphology of the synthesized pure ZnO and Ag–Ni doped ZnO NPs was characterized by powder X-ray diffraction, scanning electron microscopy (SEM), and high resolution transmission electron microscopy (HRTEM) analysis. The presence of spherical-like morphologies was confirmed from SEM and HRTEM analysis. The presence of Ni–O and Zn–O bands in the synthesized materials was found by Fourier transform infrared (FTIR) spectroscopy analysis. The MB dye was degraded under UV-light exposure in various pH conditions. The Ag (0.02%)–Ni doped ZnO NPs exhibits highest photocatalytic activity of 77% under pH 4.

Synthesis of Multi-walled Carbon Nanotubes Decorated with ZnO/Ag Nanoparticles by Co-precipitation Method

2020 ◽  
Vol 10 (2) ◽  
pp. 127-133 ◽  
Author(s):  
Duha S. Ahmed ◽  
Mohammad R. Mohammed ◽  
Mustafa K.A. Mohammed
Keyword(s):  
Carbon Nanotubes ◽  
Raman Spectra ◽  
Zno Nanoparticles ◽  
Ag Nanoparticles ◽  
Precipitation Method ◽  
Zno Nps ◽  
Eds Analysis ◽  
Multi Walled Carbon Nanotubes ◽  
Doped Zno ◽  
Co Precipitation

Background: This research indicated that such abstract are more informative and more readable, in field of preparation of nanocomposite materials. Aim: The purpose of this work represented by decoration of Carbon Nanotubes (CNTs) with nanoparticles using co-precipitation method and exhibit different physical properties from those of CNTs alone and its appropriate for this particular journal. Methods: Preparation MWCNTs surface by Ag/ZnO nanoparticles using two steps represented by acid treatment of MWCNTs in a mixture acid of sulfuric acid (95% H2SO4) and nitric acid (65% HNO3) at 3:1 ratio and second step represented by decoration of Ag/ZnO nanoparticles on FMWCNTs using co-precipitation method to prepare ZnO/Ag nanoparticles decorated on F-MWCNTs as nanocomposite material. Results: The results of this work reveal the decoration of Ag-doped ZnO nanoparticles on the FMWCNTs was achieved without any impurities as shown in XRD, Raman spectra and FTIR and FESEM observations reveal that Ag-doped ZnO nanoparticles have spherical morphologies and adhered on the functionalized MWCNTs, with diameters are about 22-30 nm. Also it is clear that there were no any other materials on the surface of F-MWCNTs except ZnO and Ag which verifies the results obtained from XRD and EDS analysis. Conclusion: In this article, Ag-doped ZnO nanoparticles have been successfully decorated on to modified MWCNTs by an in-situ co-precipitation method. From XRD results, it can be seen that the (002) peak of MWCNTs slightly increased after the addition of Ag-doped ZnO nanoparticles. Raman spectra and FTIR analysis confirmed the formation of Zn-C or Zn-O-C bonds between acid-treated MWCNTs and Ag-doped zinc oxide. The FESEM and EDS analysis revealed that the decoration of Ag-doped ZnO nanoparticles on the F-MWCNTs was achieved without any impurities. Finally, the small sizes Agdoped ZnO NPs deposited on F-MWCNTs make it very promising for biomedicine applications.

scholarly journals Multi-band visible photoresponse study of Co2+ doped ZnO nanoparticles

RSC Advances ◽  
2017 ◽  
Vol 7 (63) ◽  
pp. 39657-39665 ◽  
Author(s):  
Anju Anna Jacob ◽  
L. Balakrishnan ◽  
K. Shambavi ◽  
Z. C. Alex
Keyword(s):  
Zno Nanoparticles ◽  
Precipitation Method ◽  
Cobalt Doping ◽  
Characteristic Analysis ◽  
Visible Absorption ◽  
Doped Zno ◽  
Co Precipitation ◽  
Multi Band

Cobalt doping enhances visible absorption in ZnO nanoparticles as a result of d–d transitions. By co-precipitation method, Zn1−xCoxO nanoparticles had been synthesised and multiband photodetectors were fabricated after characteristic analysis.

Magnetism in Mn-doped ZnO nanoparticles prepared by a co-precipitation method

2006 ◽  
Vol 17 (5) ◽  
pp. 1278-1285 ◽  
Author(s):  
O D Jayakumar ◽  
H G Salunke ◽  
R M Kadam ◽  
Manoj Mohapatra ◽  
G Yaswant ◽  
...  
Keyword(s):  
Zno Nanoparticles ◽  
Precipitation Method ◽  
Doped Zno ◽  
Co Precipitation ◽  
Mn Doped

Photocatalytic Activity of Zeolite Supported Transition Metal-(Co2+ and Cr2+) Doped ZnO: Comparative Study

2015 ◽  
Vol 827 ◽  
pp. 43-48
Author(s):  
Annisa Noorhidayati ◽  
Mia Putri Rahmawati ◽  
Nadia Febiana Djaja ◽  
Rosari Saleh
Keyword(s):  
Transition Metal ◽  
Zno Nanoparticles ◽  
Diffuse Reflectance Spectroscopy ◽  
Uv Light ◽  
Transition Metal Ions ◽  
Precipitation Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
Doped Zno ◽  
Co Precipitation

Transition metal ions (Co and Cr) doped ZnO nanoparticles supported on natural zeolite were synthesized using co-precipitation method. The synthesized samples were characterized by means of X-ray diffraction, energy dispersive X-ray, Fourier-transform infrared absorption, and UV-visible diffuse reflectance spectroscopy. The samples were further used as photocatalyst for degradation of methyl orange and methylene blue in aqueous solutions under UV light irradiation. The results showed that zeolite supported Cr-doped ZnO nanoparticles is more efficient compared with zeolite supported Co-doped ZnO nanoparticles. It is also revealed that zeolite supported samples possessed higher photocatalytic efficiency compared to bare samples.

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