An Alternative Crystal Structure of Yb26B12O57 – X-Ray Structure Determination on Flux-synthesized Single Crystals
2014 ◽
Vol 69
(3)
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pp. 294-298
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Keyword(s):
Transparent and colorless single crystals of Yb26B12O57 were obtained by reacting Yb2O3 and B powder at 1000 °C in the presence of a KCl flux for 24 h in silica-jacketed Nb ampoules and subsequent removal of the flux by washing with water. Yb26B12O57 crystallizes in the monoclinic space group C2/m (no. 12, Z = 1) with the lattice parameters a = 2454:1(3), b = 357:78(4), c = 1426:7(2) pm and β = 115:111(6)°, and its structure differs slightly from that of a known compound with the same stoichiometry. Raman spectra of single crystals of the title compound were recorded and compared to those of known borate compounds
1995 ◽
Vol 50
(1)
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pp. 66-70
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Keyword(s):
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1981 ◽
Vol 36
(10)
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pp. 1208-1210
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2015 ◽
Vol 70
(3)
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pp. 191-196
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Keyword(s):
1996 ◽
Vol 51
(11)
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pp. 1583-1586
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1993 ◽
Vol 48
(7)
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pp. 1009-1012
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