scholarly journals Application of surface plasmon resonance of citrate capped silver nanoparticles for the selective determination of some fluoroquinolone drugs

2014 ◽  
Vol 116 ◽  
pp. 206-215 ◽  
Author(s):  
Hellen S. Santos ◽  
Gabriela M. de França ◽  
Eric C. Romani ◽  
Dunieskys G. Larrudé ◽  
Alessandra L.M.C. da Cunha ◽  
...  

2018 ◽  
Vol 2018 ◽  
pp. 1-9 ◽  
Author(s):  
Marwa R. El-Zahry

This contribution describes a simple, fast, and sensitive application of localized surface plasmon resonance effect of silver nanoparticles for simultaneous determination of antihypertensive drugs’ mixture atenolol and amiloride in both pharmaceutical dosage forms and in biological samples (urine). Silver nanoparticles were prepared by chemical reduction of silver nitrate using hydroxylamine HCL in an alkaline medium. Application of silver-hydroxylamine nanoparticles (SH NPs) provides many advantages including reproducibility, sensitivity, and cost effective way of analyte determination. Amiloride has four amino groups which act as attachment points on the surface of silver nanoparticles resulting in a synergistic effect on the absorption intensity of atenolol, leading to increase the sensitivity of the determination of both compounds. This method shows excellent advantages comparing with the previously reported methods, including accuracy, precision, and selectivity. The linear range of atenolol is 1 × 10−5–1 × 10−4 mol·L−1 and of amiloride is 1 × 10−6–1 × 10−5 mol·L−1. The limit of detection (LOD) values of atenolol and amiloride are 0.89 × 10−5 and 0.42 × 10−6 mol·L−1, respectively.


2020 ◽  
Vol 2 (1) ◽  
pp. 5-18
Author(s):  
Magda Mohamed Ayad Ayad ◽  
Hisham Ezzat Abdellatef ◽  
Mervat Mohamed Hosny ◽  
Naglaa Abdel-Sattar Kabil

The Analyst ◽  
2016 ◽  
Vol 141 (6) ◽  
pp. 1912-1917 ◽  
Author(s):  
Elizaveta Ermakova ◽  
Oleg Raitman ◽  
Alexander Shokurov ◽  
Maria Kalinina ◽  
Sofiya Selector ◽  
...  

An innovative design of reusable SPR chips allowing the quantitative and selective determination of mercury(ii) at the ppt level is reported.


Sign in / Sign up

Export Citation Format

Share Document