Rapid screening of 35 new psychoactive substances by ion mobility spectrometry (IMS) and direct analysis in real time (DART) coupled to quadrupole time-of-flight mass spectrometry (QTOF-MS)

2015 ◽  
Vol 7 (10) ◽  
pp. 884-893 ◽  
Author(s):  
Seongshin Gwak ◽  
Jose R. Almirall
Keyword(s):  
Mass Spectrometry ◽  
Real Time ◽  
Ion Mobility Spectrometry ◽  
Ion Mobility ◽  
Time Of Flight ◽  
Direct Analysis ◽  
Rapid Screening ◽  
New Psychoactive Substances ◽  
Psychoactive Substances ◽  
Flight Mass Spectrometry

scholarly journals Thermal Properties, Isothermal Decomposition by Direct Analysis in Real-Time-Of-Flight Mass Spectrometry and Non Isothermal Crystallization Kinetics of Poly(Ethylene-Co-Vinyl Alcohol)/Poly(ε-Caprolactone) Blend

Crystals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 292
Author(s):  
Abdulaziz Ali Alghamdi ◽  
Hussain Alattas ◽  
Waseem Sharaf Saeed ◽  
Abdel-Basit Al-Odayni ◽  
Ahmed Yacine Badjah Hadj Ahmed ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Real Time ◽  
Crystallization Kinetics ◽  
Isothermal Crystallization ◽  
Vinyl Alcohol ◽  
Time Of Flight ◽  
Direct Analysis ◽  
Isothermal Crystallization Kinetics ◽  
Flight Mass Spectrometry ◽  
Poly Ethylene

A series of poly(ethylene-co-vinyl alcohol)/poly(ε-caprolactone) blends with different compositions were prepared using solvent casting. The miscibility of this pair of polymers was investigated using differential scanning calorimetry (DSC), and proved by a negative Flory interaction parameter value calculated from the Nishi–Wang equation. The miscibility of this blend was also confirmed by scanning electronic microscopy (SEM). The thermal behaviors of the obtained materials were investigated by DSC, thermogravimetric analysis, and direct analysis in real-time–time-of-flight mass spectrometry and the results obtained were very relevant. Furthermore, the crystalline properties of the obtained materials were studied by DSC and X-ray diffraction where the Ozawa approach was adopted to investigate the non-isothermal crystallization kinetics. The results obtained revealed that this approach described the crystallization process well.

Selective reagent ionisation-time of flight-mass spectrometry: a rapid technology for the novel analysis of blends of new psychoactive substances

2015 ◽  
Vol 50 (2) ◽  
pp. 427-431 ◽  
Author(s):  
Matteo Lanza ◽  
W. Joe Acton ◽  
Philipp Sulzer ◽  
Kostiantyn Breiev ◽  
Simone Jürschik ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Time Of Flight ◽  
New Psychoactive Substances ◽  
The Novel ◽  
Psychoactive Substances ◽  
Flight Mass Spectrometry ◽  
Selective Reagent

scholarly journals Rapid determination of N-methylpyrrolidine in cefepime by combining direct infusion electrospray ionisation-time-of-flight mass spectrometry with field asymmetric waveform ion mobility spectrometry

2015 ◽  
Vol 7 (1) ◽  
pp. 34-39 ◽  
Author(s):  
Robert W. Smith ◽  
Lisa B. Cox ◽  
Aswandi Yudin ◽  
James C. Reynolds ◽  
Mark Powell ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Ion Mobility Spectrometry ◽  
Ion Mobility ◽  
Rapid Determination ◽  
Time Of Flight ◽  
Asymmetric Waveform ◽  
Direct Infusion ◽  
Electrospray Ionisation ◽  
Flight Mass Spectrometry

FAIMS separation prior to mass spectrometry enables selective transmission of NMP in cefepime without interference from NMP formed by in-source CID.

Ionization characteristics of glycosides by direct analysis in real time quadrupole-time of flight mass spectrometry

2017 ◽  
Vol 41 (3) ◽  
pp. 1103-1109 ◽  
Author(s):  
Hongmei Yang ◽  
Ge Gao ◽  
Yihan Wang ◽  
Jinrong Liu ◽  
Zongjun Li ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Real Time ◽  
Time Of Flight ◽  
Direct Analysis ◽  
Molecular Ion ◽  
Ion Formation ◽  
Flight Mass Spectrometry

Glycosides were ionized via various different reactions including (de)protonation, molecular ion formation, ISD fragmentation, and the formation of adducts.

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