Rapid screening of abused drugs by direct analysis in real time (DART) coupled to time-of-flight mass spectrometry (TOF-MS) combined with ion mobility spectrometry (IMS)

2017 ◽  
Vol 279 ◽  
pp. 268-280 ◽  
Author(s):  
Ru Lian ◽  
Zhongping Wu ◽  
Xiaobao Lv ◽  
Yulan Rao ◽  
Haiyang Li ◽  
...  
RSC Advances ◽  
2016 ◽  
Vol 6 (107) ◽  
pp. 105780-105785 ◽  
Author(s):  
Xing Fan ◽  
Chu-Fan Wang ◽  
Chun-Yan You ◽  
Xian-Yong Wei ◽  
Lu Chen ◽  
...  

Direct analysis in real time ionization technique coupled with a quadrupole time-of-flight mass spectrometry (Q-TOF MS) was applied to characterize raw coal and coal derivatives in the solid state.


Crystals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 292
Author(s):  
Abdulaziz Ali Alghamdi ◽  
Hussain Alattas ◽  
Waseem Sharaf Saeed ◽  
Abdel-Basit Al-Odayni ◽  
Ahmed Yacine Badjah Hadj Ahmed ◽  
...  

A series of poly(ethylene-co-vinyl alcohol)/poly(ε-caprolactone) blends with different compositions were prepared using solvent casting. The miscibility of this pair of polymers was investigated using differential scanning calorimetry (DSC), and proved by a negative Flory interaction parameter value calculated from the Nishi–Wang equation. The miscibility of this blend was also confirmed by scanning electronic microscopy (SEM). The thermal behaviors of the obtained materials were investigated by DSC, thermogravimetric analysis, and direct analysis in real-time–time-of-flight mass spectrometry and the results obtained were very relevant. Furthermore, the crystalline properties of the obtained materials were studied by DSC and X-ray diffraction where the Ozawa approach was adopted to investigate the non-isothermal crystallization kinetics. The results obtained revealed that this approach described the crystallization process well.


2015 ◽  
Vol 7 (1) ◽  
pp. 34-39 ◽  
Author(s):  
Robert W. Smith ◽  
Lisa B. Cox ◽  
Aswandi Yudin ◽  
James C. Reynolds ◽  
Mark Powell ◽  
...  

FAIMS separation prior to mass spectrometry enables selective transmission of NMP in cefepime without interference from NMP formed by in-source CID.


2017 ◽  
Vol 41 (3) ◽  
pp. 1103-1109 ◽  
Author(s):  
Hongmei Yang ◽  
Ge Gao ◽  
Yihan Wang ◽  
Jinrong Liu ◽  
Zongjun Li ◽  
...  

Glycosides were ionized via various different reactions including (de)protonation, molecular ion formation, ISD fragmentation, and the formation of adducts.


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