Thermal stress and strain effects on phase transition temperatures in differential thermal analysis testing

1992 ◽  
Vol 23 (2) ◽  
pp. 451-455 ◽  
Author(s):  
Y. T. Zhu ◽  
J. H. Devletian
2000 ◽  
Vol 55 (11-12) ◽  
pp. 899-901
Author(s):  
Mirnaya T. A. ◽  
L. S. Sudovtsova ◽  
G. G. Yaremchuk

Abstract The phase transition temperatures were determined by differential thermal analysis and hot stage polarization microscopy between room temperature and the isotropic liquid region for the binary systems of lead (II) decanoate with zinc (II) or cadmium (II) decanoate. The boundaries of the liquid crystal formation in these systems were found.


2016 ◽  
Vol 165 ◽  
pp. 11-19 ◽  
Author(s):  
Yunna Sun ◽  
Shi Sun ◽  
Yazhou Zhang ◽  
Jiangbo Luo ◽  
Yan Wang ◽  
...  

2017 ◽  
Vol 62 (4) ◽  
pp. 1945-1955
Author(s):  
A. Dębski ◽  
B. Onderka ◽  
W. Gąsior ◽  
T. Gancarz

AbstractWith the use of the differential thermal analysis (DTA), studies of the phase transitions were conducted for 90 of alloys from the quaternary Bi-In-Sn-Zn system and for the constant ratio of Bi:In and Bi:Sn. The studies were conducted for the alloys prepared from the purity metals (Bi, In, Sn, Zn = 99.999 mas. %) by way of melting in a graphite crucible in a glove-box filled with Ar, in which the impurities level was less than 0.1 ppm. After melting and thorough mixing, the liquid alloys were poured out into a graphite test mold. The phase transition temperature data obtained from the DTA investigations were next confronted with those determined from the calculations based on the binary and ternary optimized thermodynamic parameters available in the literature. It was found that the experimental and the calculated phase transition temperatures were in good agreement.


RSC Advances ◽  
2021 ◽  
Vol 11 (29) ◽  
pp. 17622-17629
Author(s):  
Ae Ran Lim

We studied the thermal behavior and structural dynamics of [NH3(CH2)3NH3]CdBr4 near phase transition temperatures.


2021 ◽  
Author(s):  
Dongdong Lu ◽  
Mingning Zhu ◽  
Jing Jin ◽  
Brian R. Saunders

Thermally- and pH-responsive microgels (MGs) and hydrogels are fascinating network systems that have been applied in biomedical engineering and sensing. The volume-swelling ratio (Q) and the volume-phase transition temperatures (VPTTs)...


1992 ◽  
Vol 7 (8) ◽  
pp. 2035-2039 ◽  
Author(s):  
T.G. Holesinger ◽  
D.J. Miller ◽  
S. Fleshler ◽  
L.S. Chumbley

Reactions with alumina and platinum crucibles were studied during the preparation of Bi2Sr2Ca1Cu2Oy “2212” glasses. In particular, reactions with Al2O3 are of interest since alumina is a potential substrate material in applications of this superconductor. Glasses processed using alumina crucibles were completely homogeneous and free of secondary phases although the material contained 2.26 at. % Al in solution. After heat treatments, Al was found in the form of SrCaAlOy particles located primarily along grain boundaries of the 2212 superconducting phase. Platinum contamination was minimal (<0.02 at. %) and no Pt-containing secondary phases were found in amorphous or annealed samples. Glasses made with Pt crucibles were found to contain small amounts of CaO, Sr14−xCaxCu24O41, and 2201 as second phases. Differential thermal analysis (DTA) suggested that the crystallization processes were essentially the same for all samples although the small amount of Al seemed to slow the kinetics leading to the formation of 2212. Neither Al nor Pt was detected within the 2212 phase. The measured superconducting compositions in each annealed sample were nearly the same with identical transition temperatures of 88 K. Overall differences in stoichiometry were accommodated by changes in the number and composition of the secondary phases present.


AIP Advances ◽  
2018 ◽  
Vol 8 (5) ◽  
pp. 056428 ◽  
Author(s):  
Shivakumar G. Hunagund ◽  
Shane M. Harstad ◽  
Ahmed A. El-Gendy ◽  
Shalabh Gupta ◽  
Vitalij K. Pecharsky ◽  
...  

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