High resolution magic angle spinning NMR studies of31P and11B in fast ion conducting AgI-Ag2O-P2O5 and AgI-Ag2O-B2O3 glasses

Pramana ◽  
1989 ◽  
Vol 32 (6) ◽  
pp. 811-820 ◽  
Author(s):  
M C R Shastry ◽  
K J Rao
Keyword(s):  
High Resolution ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Nmr Studies ◽  
Ion Conducting ◽  
Angle Spinning ◽  
Fast Ion

scholarly journals High-resolution magic angle spinning NMR studies for metabolic characterization of Arabidopsis thaliana mutants with enhanced growth characteristics

PLoS ONE ◽  
2018 ◽  
Vol 13 (12) ◽  
pp. e0209695 ◽  
Author(s):  
Dieuwertje Augustijn ◽  
Niels van Tol ◽  
Bert J. van der Zaal ◽  
Huub J. M. de Groot ◽  
A. Alia
Keyword(s):  
Arabidopsis Thaliana ◽  
High Resolution ◽  
Magic Angle Spinning ◽  
Growth Characteristics ◽  
Magic Angle ◽  
Nmr Studies ◽  
Angle Spinning

scholarly journals General Guidelines for Sample Preparation Strategies in HR-µMAS NMR-based Metabolomics of Microscopic Specimens

Metabolites ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 54 ◽  
Author(s):  
Lucas-Torres ◽  
Bernard ◽  
Huber ◽  
Berthault ◽  
Nishiyama ◽  
...  
Keyword(s):  
High Resolution ◽  
Sample Preparation ◽  
Bulk Sample ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Nmr Studies ◽  
Sample Rotation ◽  
Angle Spinning ◽  
Bioanalytical Techniques ◽  
General Studies

The study of the metabolome within tissues, organisms, cells or biofluids can be carried out by several bioanalytical techniques. Among them, nuclear magnetic resonance (NMR) is one of the principal spectroscopic methods. This is due to a sample rotation technique, high-resolution magic angle spinning (HR-MAS), which targets the analysis of heterogeneous specimens with a bulk sample mass from 5 to 10 mg. Recently, a new approach, high-resolution micro-magic angle spinning (HR-μMAS), has been introduced. It opens, for the first time, the possibility of investigating microscopic specimens (<500 μg) with NMR spectroscopy, strengthening the concept of homogeneous sampling in a heterogeneous specimen. As in all bioanalytical approaches, a clean and reliable sample preparation strategy is a significant component in designing metabolomics (or -omics, in general) studies. The sample preparation for HR-μMAS is consequentially complicated by the μg-scale specimen and has yet to be addressed. This report details the strategies for three specimen types: biofluids, fluid matrices and tissues. It also provides the basis for designing future μMAS NMR studies of microscopic specimens.

Multinuclear Solid-State High-Resolution and13C -{27Al} Double-Resonance Magic-Angle Spinning NMR Studies on Aluminum Alkoxides

2006 ◽  
Vol 110 (13) ◽  
pp. 6553-6560 ◽  
Author(s):  
Anuji Abraham ◽  
Roel Prins ◽  
Jeroen A. van Bokhoven ◽  
Ernst R. H. van Eck ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Double Resonance ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Nmr Studies ◽  
Angle Spinning

High Resolution Magic Angle Spinning NMR in Combinatorial Chemistry

2001 ◽  
Vol 4 (4) ◽  
pp. 333-351 ◽  
Author(s):  
G. Lippens ◽  
R. Warrass ◽  
J. Wieruszeski ◽  
P. Rousselot-Pailley ◽  
G. Chessari
Keyword(s):  
High Resolution ◽  
Combinatorial Chemistry ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning
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