Compression Texture of Iodide Titanium

JOM ◽  
1952 ◽  
Vol 4 (6) ◽  
pp. 615-618
Author(s):  
D. N. Williams ◽  
D. S. Eppelsheimer

Author(s):  
E. U. Lee ◽  
P. A. Garner ◽  
J. S. Owens

Evidence for ordering (1-6) of interstitial impurities (O and C) has been obtained in b.c.c. metals, such as niobium and tantalum. In this paper we report the atomic and microstructural changes in an oxygenated c.p.h. metal (alpha titanium) as observed by transmission electron microscopy and diffraction.Oxygen was introduced into zone-refined iodide titanium sheets of 0.005 in. thickness in an atmosphere of oxygen and argon at 650°C, homogenized at 800°C and furnace-cooled in argon. Subsequently, thin foils were prepared by electrolytic polishing and examined in a JEM-7 electron microscope, operated at 100 KV.



Author(s):  
D.M. Vanderwalker

There is a fundamental interest in electrochemical fusion of deuterium in palladium and titanium since its supposed discovery by Fleischmann and Pons. Their calorimetric experiments reveal that a large quantity of heat is released by Pd after hours in a cell, suggesting fusion occurs. They cannot explain fusion by force arguments, nor can it be an exothermic reaction on the formation of deuterides because a smaller quantity of heat is released. This study examines reactions of deuterium in titanium.Both iodide titanium and 99% pure titanium samples were encapsulated in vacuum tubes, annealed for 2h at 800 °C. The Ti foils were charged with deuterium in a D2SO4 D2O solution at a potential of .45V with respect to a calomel reference junction. Samples were ion beam thinned for transmission electron microscopy. The TEM was performed on the JEOL 200CX.The structure of D charged titanium is α-Ti with hexagonal and fee deuterides.



1958 ◽  
Vol 8 (1) ◽  
pp. 94-99 ◽  
Author(s):  
Karel Toman ◽  
Marie Simerská


1958 ◽  
Vol 29 (7) ◽  
pp. 1130-1131 ◽  
Author(s):  
Allan M. Russell ◽  
Robert C. Abbott


JOM ◽  
1952 ◽  
Vol 4 (8) ◽  
pp. 843-847 ◽  
Author(s):  
O. J. C. Runnalls ◽  
L. M. Pidgeon
Keyword(s):  


2021 ◽  
Vol 1035 ◽  
pp. 63-71
Author(s):  
Bei Bei Dong ◽  
Zhi Min Zhang ◽  
Jian Min Yu ◽  
Xin Che

In order to determine the deformation temperature of next pass, the hot compression tests were performed by Gleeble-3800 at different temperature form 380 to 420 °C. The microstructure and texture evolution of repetitive upsetting-extruded (RUEed) Mg-Gd-Y-Zn-Zr alloy during hot compression were studied by electron backscattering diffraction (EBSD) analysis. The results showed that the dynamic recrystallization (DRX) occured during the hot compression processing from the strain-stress flow curves. When the temperature increased to 420 °C, the average grain size reduced to 6.64 μm, and the volume fraction of DRXed grains increased to 81.5%. All the compressed alloys exhibited a typical compression texture, the maximum texture intensity of {0001} plane gradually decreased with increasing temperature. When the compression temperature was up to 420°C, the the maximum texture intensity of {0001} plane was 3.207 due to the effect of DRXed grains. Finally, 420°C is chosen as the next deformation of next pass because of the more precipitation and DRXed grains.



1981 ◽  
Vol 12 (2) ◽  
pp. 133-139 ◽  
Author(s):  
PETER W. VOISEY ◽  
M. KLOEK


1991 ◽  
Vol 14 ◽  
pp. 377-381
Author(s):  
H.-G. Brokmeier




JOM ◽  
1953 ◽  
Vol 5 (1) ◽  
pp. 57-61 ◽  
Author(s):  
Carl J. McHargue ◽  
Joseph P. Hammond
Keyword(s):  


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