scholarly journals Dual-frequency ultrasonic cleaning with diluted phosphoric acid solution for removing oxide scale of uncoated steel sheets in hot stamping

Author(s):  
Naotaka Nakamura ◽  
Ken-ichiro Mori ◽  
Tsuyoshi Komatsu ◽  
Takafumi Hayashi ◽  
Takayuki Suzuki ◽  
...  

AbstractDual-frequency ultrasonic cleaning with a diluted phosphoric acid solution was developed to remove oxide scales on surfaces of hot-stamped parts from uncoated steel sheets, and conventional shot blasting processes are omitted. The removal of the oxide scale by ultrasonic cleaning is accelerated by the phosphoric acid solution and the dual frequency. The removing time for the phosphoric acid solution was shorter than that for a hydrochloric acid solution, and rust appearing for leaving after cleaning was prevented by generating an iron phosphate layer. In dual-frequency ultrasonic cleaning with the diluted phosphoric acid solution, the oxide scale was dissolved, and then the oxide scales were exfoliated from the thin scale and high-pressure portions. The removing time decreased with decreasing pH and oxide scale thickness and with increasing solution temperature. The surface roughness and distortion of an ultrasonic-cleaned hot-stamped part were smaller than those for shot blasting, and the weldability and paintability were similar. The oxide scale of a hot-stamped part having a nonuniform distribution of oxide scale thickness was successfully removed by dual-frequency ultrasonic cleaning with the diluted phosphoric acid solution.

1978 ◽  
Vol 7 (4) ◽  
pp. 313-318 ◽  
Author(s):  
I.A.S. Mansour ◽  
G.H. Sedahmed ◽  
M.Z. El-Abd ◽  
A.M. Ahmed

2018 ◽  
Vol 65 (5) ◽  
pp. 506-514 ◽  
Author(s):  
Khalid Rashid ◽  
Anees Khadom

PurposeThe purpose of this study is to investigate the corrosion inhibition of mild steel alloy in 2 M H3PO4solution by the pomegranate peel extract as a friendly inhibitor was studied at various temperatures, inhibitor concentrations and immersion times.Design/methodology/approachA weight loss method was used to evaluate the corrosion rate. The experimental Taguchi design method was used for the distribution of experiments. The experimental design gave results which were impossible to show graphically. However, this problem was solved effectively with the aid of regression analysis.FindingsCorrosion rate increased with temperature according to Arrhenius equation. It was found that the efficiency of inhibition was increased with an increase in the concentration of inhibitor and immersion time. However, this diminishes with increased temperature. According to Langmuir isotherm, the inhibitor was adsorbed physically on steel surface. The negative sign of estimated heat of adsorption suggests a stable spontaneous inhibition process. Combination of mathematical and statistical analysis was proposed to demonstrate the results of corrosion rate with high correlation coefficients. In addition, Fourier transform infrared spectrometer examinations confirmed that the organic inhibitor consists of phenolic components as main materials.Originality/valueUsing unconventional approach for evaluation of environmentally friendly inhibitor for corrosion of mild steel in phosphoric acid solution.


2019 ◽  
Vol 87 (1) ◽  
pp. 14-19 ◽  
Author(s):  
Lifeng DING ◽  
Peng WU ◽  
Jun CHENG ◽  
Yulan NIU ◽  
Zhengwei SONG ◽  
...  

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