Effects of isothermal crystallization on fracture toughness and crack growth behavior of poly (lactic acid)

2005 ◽  
Vol 40 (4) ◽  
pp. 1055-1058 ◽  
Author(s):  
SANG-DAE PARK ◽  
MITSUGU TODO ◽  
KAZUO ARAKAWA
2004 ◽  
Vol 261-263 ◽  
pp. 105-110 ◽  
Author(s):  
Sang Dae Park ◽  
Mitsugu Todo ◽  
Kazuo Arakawa

Effect of annealing on the fracture behavior of poly(lactic acid) (PLA) was investigated. Fracture toughness of PLA samples prepared under different annealing conditions was measured under static and dynamic loadings. Microstructure and crack growth behavior were characterized by polarizing microscopy (POM). Crystallinity was determined by DSC analysis. Fracture surface morphology was also studied by scanning electron microscopy. It was shown that the static fracture toughness increased with increase of crystallinity, while the dynamic toughness increased as crystallinity increased. POM exhibited that craze formation played an important role in the fracture mechanism of amorphous samples. Macroscopic fracture toughness and microscopic crack growth mechanism were correlated on the basis of these experimental results, and effect of annealing on the toughness and mechanism were discussed.


JOM ◽  
2015 ◽  
Vol 67 (10) ◽  
pp. 2288-2295 ◽  
Author(s):  
Mohsen Seifi ◽  
Dongyue Li ◽  
Zhang Yong ◽  
Peter K. Liaw ◽  
John J. Lewandowski

2016 ◽  
Vol 139 (1) ◽  
Author(s):  
Tarek M. A. A. EL-Bagory ◽  
Maher Y. A. Younan

The behavior of crack growth of polymeric materials is affected by several operating conditions such as crosshead speed, specimen thickness, load line, and specimen configurations, which reverse the behavior of crack from stable to unstable crack growth behavior. The main objective of the present paper is the determination of plane strain fracture toughness (KIC) for polyvinyl chloride (PVC) used in piping water transmission systems. The dimensions of the PVC pipe are outside diameter, Do = 315 mm, standard dimensions ratio, SDR = 13.23, ratio between outside to inside radii Ro/Ri = 1.179, and pipe thickness, t = 24 mm. Curved specimens are prepared from a pipe by cutting 12 mm thickness ring segments. The curved specimens are divided into two specimen configurations, namely, curved three-point bend (CTPB) and C-shaped tension (CST) specimens. All specimens are provided artificially with a precrack. CTPB specimen is further cut into five 72 deg sectors with each being centrally notched to a depth approximately a = 0.479 of the wall thickness. CST specimen configuration is characterized by the eccentricity X = 0, and 0.5 W, of the loading holes from the bore surface. The linear elastic fracture mechanics theory (LEFM) is used to predict the plane strain fracture. The tests are carried out at room temperature, Ta equal 20 °C, and different crosshead speeds of (10–500 mm/min). The numerical analysis carried out within the frame of the present work is done using the finite element program Cosmos 2.6. Finite element method (FEM) is used to compute the stress intensity factor KQ surrounding the crack tip. The computed stress intensity factor can then be compared with that obtained by theoretical equation. The experimental fracture test results reveal that the crosshead speed has been proven to affect the mode of failure and mode of fracture. At lower crosshead speeds, the mode of failure is ductile, while at higher crosshead speeds, it is brittle. The specimen configuration also affects the fracture toughness. CST specimens show higher fracture toughness in the case of pin loading location X = 0.5W than X = 0 by about (12%). The transitional crosshead speed is affected by specimen geometry. CST specimens (CST) at X = 0 and 0.5W have higher transitional crosshead speed compared with the CTPB specimen configuration.


2016 ◽  
Vol 715 ◽  
pp. 116-121 ◽  
Author(s):  
Sota Oshima ◽  
Hisayoshi Ishida ◽  
Ryota Tanegashima ◽  
Takayuki Kusaka ◽  
Tomo Takeda

A novel experimental method has been developed to evaluate the mode I crack growth behavior of adhesively bonded joints under impact loading. The split Hopkinson pressure bar (SHPB) technique and the digital image correlation (DIC) technique was employed to evaluate the crack growth behavior. To reduce the dynamic effects by controlling loading input of the SHPB apparatus, the fracture toughness was determined precisely based on static evaluation formula. To contrive the testing set-up, high loading rate was kept until the arrest of crack. The fracture toughness of titanium alloy/epoxy adhesively bonded joints during crack propagation was obtained successfully by using present method.


Materials ◽  
2021 ◽  
Vol 14 (21) ◽  
pp. 6621
Author(s):  
Qingyan Zhu ◽  
Peng Zhang ◽  
Xingdong Peng ◽  
Ling Yan ◽  
Guanglong Li

The fatigue crack growth behavior and fracture toughness of EH36 thermo-mechanical control process (TMCP) steel were investigated by fatigue crack growth rate testing and fracture toughness testing at room temperature. Scanning electron microscopy was used to observe the fracture characteristics of fatigue crack propagation and fracture toughness. The results indicated that the microstructure of EH36 steel is composed of ferrite and pearlite with a small amount of texture. The Paris formula was obtained based on the experimental data, and the value of fracture toughness for EH36 steel was also calculated using the J-integral method. The observations conducted on fatigue fracture surfaces showed that there were a lot of striations, secondary cracks and tearing ridges in the fatigue crack propagation region. Additionally, there existed many dimples on the fracture surfaces of the fracture toughness specimens, which indicated that the crack was propagated through the mechanism of micro-void growth/coalescence. Based on the micromechanical model, the relationship between the micro-fracture surface morphology and the fracture toughness of EH36 steel was established.


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