Microstructure and Fracture Toughness of Nitrided D2 Steels Using Potential-Controlled Nitriding

Potential-controlled nitriding is an effective technique for enhancing the life of steel molds and dies by improving their surface hardness and toughness against fatigue damage. In this study, the effect of the nitriding potential on the microstructure and fracture toughness of nitrided AISI D2 steels was investigated. The nitrided layers were characterized by microhardness measurements, optical microscopy, and scanning electron microscopy, and their phases were identified by X-ray and electron backscatter diffraction. As the nitriding potential increased to 2.0 atm−1/2, an increase in the surface hardness and fracture toughness was observed with the growth of the compound layer. However, both the surface hardness and the fracture toughness decreased at the higher nitriding potential of 5.0 atm−1/2 owing to the increased porosity in the compound layers, which mainly consist of the ε (Fe2–3N) phase. Additionally, by observing crack growth behavior, the fracture toughness was analyzed considering the material characteristics of the diffusion and compound layers. The fracture toughness was influenced by the location of the initial Palmqvist cracks due to the localized plastic deformation of the diffusion layer and increased crack length due to the porous compound layer.

Conductivity, microstructure and mechanical properties of tape-cast LATP with LiF and SiO2 additives

LATP sheets with LiF and SiO2 addition prepared by tape cast as electrolytes for solid-state batteries were characterized regarding conductivity, microstructure and mechanical properties aiming toward an optimized composition. The use of additives permitted a reduction of the sintering temperature. Rietveld analyses of the samples with additives revealed a phase mixture of NaSICON modifications crystallizing with rhombohedral and orthorhombic symmetry as a superstructure with space group Pbca. It seems that LiF acts as a sintering additive but also as a mineralizer for the superstructure of LATP. As general trend, higher LiF to SiO2 ratios led to lower porosities and higher values of elastic modulus and hardness determined by indentation testing, but the presence of the orthorhombic LATP leads to a decrease in the ionic conductivity. Micro-pillar testing was used to assess the crack growth behavior revealing weak grain boundaries.

Numerical Simulation of Crack Propagation of Architecture Glass Under Explosion and Impact Load

Crack initiation and propagation is a long-standing difficulty in solid mechanics, especially for elastic-brittle material. To explore the damage and crack propagation behavior of architectural glass under different type of loads, the element deletion (ED), discontinuous Galerkin peridynamics (DG-PD) and meshless peridynamics (M-PD) methods are studied. Taking the architecture glass as an example, the crack propagation behavior under the bullet impact and explosion load are studied. The JH-2 material model is used in the ED method, and the maximum principal stress and maximum principal strain failure criteria are applied at the same time. In the DG-PD method, it conducts a node separation operation and imposes the criterion of the critical energy release rate. The M-PD method adopts a self-programmed particle discretization method and imposes a criterion of critical elongation. Three methods can simulate the crack growth behavior of glass material, but the PD method has great advantages in detail, such as crack bifurcation and penetration. For low-velocity bullets, the failure behavior of glass all shows cross-shaped cracks in different methods. The splashing of elements or particles appears in the two PD methods, but the particle splashing of the M-PD method is more obvious, and the DG-PD method captures the crack bifurcation effect better. For the failure behavior of glass under explosive loading, the PD method is obviously better than the ED method in terms of modal appearance. However, in the mechanical behavior of specific elements, the two methods have a high degree of agreement.

Effect of Rod-like Structure on Fatigue Life, Short Surface Crack Initiation and Growth Characteristics of Extruded Aluminum Alloy A2024 (Analysis via Modified Linear Elastic Fracture Mechanics)

In the Al alloy A2024-T3 extruded material, a rod-like structure is generated parallel to the extrusion direction. In this study, the effects of rod-like structures on fatigue crack initiation and growth behavior were comprehensively investigated. Two types of specimens were used in a fatigue experiment, in which the direction of the load stress amplitude was parallel (specimen P) and perpendicular (specimen V) to the rod-like structure. Based on the experimental and analytical results, the following findings were obtained regarding the fatigue life, location of crack initiation, and fatigue crack growth behavior. Because the fatigue life of specimen P was longer than that of specimen V, it is inferred that the rod-like structure significantly affects the fatigue life. In specimen P, fatigue cracks were generated from the grain boundaries of the Al matrix. By contrast, in specimen V, cracks were generated from the Cu–Mg-based intermetallic compound in the Al matrix. In specimen P, fatigue cracks were more likely to propagate across the rod-like structure, which decreased the fatigue crack growth rate. In specimen V, fatigue cracks did not propagate across the rod-like structure; instead, they propagated through the Al matrix. Therefore, the fatigue crack growth resistance of specimen V was lower than that of specimen P. The relationship between the fatigue crack growth rate and the modified linear elastic fracture mechanics parameter could be used to predict the S–N curve (stress amplitude vs. fatigue life) and fatigue crack growth behavior. The predicted results agreed well with the experimental results.