Synthesis and characterization of a porous acidic catalyst functionalized with an imidazole ionic liquid, and its use for synthesis of phthalazinedione and phthalazinetrione heterocyclic compounds

2015 ◽  
Vol 41 (12) ◽  
pp. 9903-9915 ◽  
Author(s):  
Jamal Davarpanah ◽  
Parizad Rezaee ◽  
Somayeh Elahi
2019 ◽  
Vol 9 (02) ◽  
Author(s):  
Zena G. Alrecabi ◽  
Zainab Amer ◽  
Naeemah Al-Lami

This study including prepared new colored esters containing heterocyclic with high molecular weights. In the first part of work we synthesized azo dyes [1,2] from the reaction p-toluidine with β-naphthol and o-nitro phenol, thin we synthesized Schiff bases [3,4] by the reaction anthranilic acid with benzaldehyde and dimethyl benzaldehyde. The reaction azo dyes (contain OH group) with Schiff base (contain COOH group) these led to produce the new colored esters [A1-A4]. The second part of work was modification the (C=N-) group in esters to heterocyclic compounds by reacting with phenyl iso cyanide to produce new β-lactam [B1-B4] and with anthranilic acid to get new hydroquinazoline [C1-C4]. All these compounds were characterized by physical properties and spectral methods FTIR, 1H-NMR and 13C-NMR.


BioResources ◽  
2015 ◽  
Vol 10 (2) ◽  
Author(s):  
Jinmin Qin ◽  
Ziyu Qin ◽  
Xueqiong Yin ◽  
Qinghuan Zeng ◽  
Li Zhu

2012 ◽  
Vol 518-523 ◽  
pp. 3989-3992 ◽  
Author(s):  
Yang Zhang ◽  
Xiao Hua Tu ◽  
Cheng Ping Miao ◽  
Jian Yi Wu

A novel CIL of N-butyl-N-methyl imidazolium-D-(-)-tartrate has been designed and synthesized by neutralization reaction. Its structure was characterized by 1H-NMR and 13C-NMR spectra, the optical rotation was characterized by polarimeter with the value of-15.0º, and the purity was characterized by ion chromatography with the value of 98.4%.


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