Synthesis and characterization of multi–wall carbon nanotubes supported-hydrated iron phosphate cathode material for lithium–ion cells by a novel homogeneous precipitation method

AbstractBaCO3 nanoparticles with different morphologies including needle-like, rod-like, bird's nest-like and flower-like have been successfully synthesized by the microwave homogeneous precipitation method using BaCl2·2H2O, NaOH and (NH2)2CO as raw materials with the help of different guide reagents, such as citric acid (CA), sodium triphosphate (STPP) and ethylene diamine tetraacetic acid (EDTA). Their phases and morphologies were characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM), respectively. The characterization results show that different guide reagents have little effect on the phase structure and composition of products while they play significant roles in determining the morphology of products. All the synthesized BaCO3 nanoparticles have typical orthorhombic structures that are well-crystallized.

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Synthesis and characterization of nanoestructured TiO2 anatase-phase powders obtained by the homogeneous precipitation method

2013 10th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE) ◽

10.1109/iceee.2013.6676015 ◽

2013 ◽

Cited By ~ 1

Author(s):

J. Morales ◽

A. Maldonado ◽

M. de la L. Olvera

Keyword(s):

Anatase Phase ◽

Precipitation Method ◽

Synthesis And Characterization ◽

Homogeneous Precipitation ◽

Tio2 Anatase ◽

Homogeneous Precipitation Method

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Synthesis and Characterization of Hollow Magnetic Alloy (GdNi2, Co5Gd) Nanospheres Coated with Gd2O3

Journal of Nanomaterials ◽

10.1155/2014/604035 ◽

2014 ◽

Vol 2014 ◽

pp. 1-9

Author(s):

Wang Li ◽

Fa-gen Li ◽

Jun Wang ◽

Guo-meng Zhao

Keyword(s):

Large Scale ◽

Precipitation Method ◽

Synthesis And Characterization ◽

Magnetic Alloy ◽

Homogeneous Precipitation ◽

Hollow Nanospheres ◽

Magnetic Nanospheres ◽

Homogeneous Precipitation Method ◽

Potential Applications

Uniform magnetic hollow nanospheres (GdNi2, Co5Gd) coated with Gd2O3have been successfully prepared on a large scale via a urea-based homogeneous precipitation method using silica (SiO2) spheres as sacrificed templates, followed by subsequent heat treatment. Nitrogen sorption measurements and scanning electron microscope reveal that these hollow-structured magnetic nanospheres have the mesoporous shells that are composed of a large amount of uniform nanoparticles. After reduction treatment, these nanoparticles exhibit superparamagnetism that might have potential applications in medicine. Furthermore, the developed synthesis route may provide an important guidance for the preparation of other multifunctional hollow spherical materials.

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Synthesis and Characterization of Anatase TiO2 Powder using a Homogeneous Precipitation Method

Korean Journal of Metals and Materials ◽

10.3365/kjmm.2011.49.5.367 ◽

2011 ◽

Vol 49 (6) ◽

Keyword(s):

Anatase Tio2 ◽

Precipitation Method ◽

Synthesis And Characterization ◽

Homogeneous Precipitation ◽

Tio2 Powder ◽

Homogeneous Precipitation Method

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Synthesis and Characterization of Hexagonal Prismatic Ca10(PO4)6(OH)2 Prepared by Homogeneous Precipitation Method

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.391-392.1239 ◽

2011 ◽

Vol 391-392 ◽

pp. 1239-1243

Author(s):

Zhan Hui Zhang ◽

Zhi Liang Huang ◽

Jian Qiu Li ◽

Ru An Chi ◽

Yue Hua Hu ◽

...

Keyword(s):

Growth Process ◽

Crystal Morphology ◽

Precipitation Method ◽

Synthesis And Characterization ◽

Hexagonal Prism ◽

Homogeneous Precipitation ◽

X Ray Diffraction ◽

X Ray ◽

Homogeneous Precipitation Method

Hexagonal prismatic hydroxyapatite (Ca10(PO4)6(OH)2, HAP) was successfully prepared by a homogeneous precipitation method. The products were characterized by X-ray diffraction, Fourier transform infrared spectrum, and scanning electron microscope. The growth process of the hexagonal prism was surveyed in detail based on the effects of the reaction time on the phase composition and the crystal morphology.

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